High-transparency caesalpinia spinosa glue as well as preparation method and application thereof

A thorn cloud solid glue and transparent technology, which is applied in the field of high transparent thorn cloud solid glue and its preparation field, can solve the problem of limiting the application range and application value of thorn cloud solid glue, and the quality characteristics of high transparent thorn cloud solid glue are not clear. , does not involve the application of high-transparency type thorn cloud solid glue and other issues, to achieve the effect of being suitable for large-scale promotion and application, unique application value, and improving comprehensive nursing effect

Active Publication Date: 2022-05-13
SHANGHAI HOPE TEC BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, commercially available tara gum is mostly imported from Peru. Due to the limitation of production and processing technology, commercially available tara gum is milky white viscous liquid after being dissolved in water. The aqueous solution of tara gum has poor clarity and light transmittance. Low, can not be directly used in the production of clarification, transparent liquid dosage form products, which restricts and limits the application range and application value of tara gum
It has not yet involved the preparation process of highly transparent tara gum, and has not clarified the quality characteristics of highly transparent tara gum, nor has it involved the application of highly transparent tara gum in cosmetics, food, and health products Research

Method used

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  • High-transparency caesalpinia spinosa glue as well as preparation method and application thereof
  • High-transparency caesalpinia spinosa glue as well as preparation method and application thereof
  • High-transparency caesalpinia spinosa glue as well as preparation method and application thereof

Examples

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preparation example Construction

[0061] The application proposes a preparation method of highly transparent tara gum, comprising the following steps:

[0062] (1) commercially available tara gum solid powder is placed in water to keep warm and fully swell, stir, disperse, and dissolve into a milky white solution;

[0063] (2) heating the milky white solution to adjust the pH value of the milky white solution, and then adding protease to the above milky white solution for enzymolysis to obtain an enzymolysis feed liquid;

[0064] (3) adjusting the pH value of the above-mentioned enzymatic hydrolysis feed liquid, heating the enzymatic hydrolysis feed liquid and then insulated to inactivate the enzyme, so as to obtain the enzymatic hydrolysis feed liquid;

[0065] (4) Carrying out column adsorption filtration to the above-mentioned enzyme-killing liquid to obtain the filtrate;

[0066] (5) The above-mentioned filtrate is subjected to fine filtration, and the pH value of the fine filtrate is adjusted to obtain a...

preparation example 1

[0112] A kind of highly transparent tara gum, comprising the following preparation steps:

[0113] (1) swelling and dissolution:

[0114] Get 5 kilograms of commercially available tara gum solid powder and place in 1000 liters of extraction tanks, quantitatively add pure water in 1000 liters of extraction tanks, the addition weight of pure water is 100 times of the tara gum feeding weight, i.e. 500 kilograms, Start stirring, heat up to 60°C, keep warm, swell, stir, disperse, and dissolve into a milky white solution.

[0115] (2) Enzymolysis:

[0116] The above-mentioned dissolving qualified tara gum solution is heated up to 60°C, and the pH value of the tara gum solution is adjusted with 5% dilute sodium hydroxide aqueous solution: 7.0, and the tara gum solution is added to the tara gum solution for feeding. 0.5% by weight of neutral protease, heat preservation and extraction for 4 hours to obtain enzymatic hydrolysis material liquid.

[0117] (3) pH adjustment, enzyme inac...

Embodiment 1

[0126] A highly transparent tara gum product for cosmetics without preservatives, comprising the following preparation steps:

[0127] (1) Preparation: add p-anisic acid in the tara gum concentrated solution obtained in Preparation Example 1, the addition of p-anisic acid is 0.05% by weight of the concentrated solution, i.e. 0.125 kg, and add propylene glycol in the concentrated solution simultaneously , the addition of propylene glycol is 5% by weight of the concentrated solution, i.e. 12.5 kilograms;

[0128] (2) Sterilization: After the preparation solution is stirred evenly, heat up to 80° C., heat preservation and sterilization for 30 minutes to obtain a sterilizing solution;

[0129] (3) Fine filtration: the sterilizing solution is passed through a 0.2 μm filter element to obtain a clear and transparent solution, which is prepared into a highly transparent tara gum product for cosmetics without preservatives.

[0130] The characteristic quality index of highly transpare...

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Abstract

The invention discloses high-transparency caesalpinia spinosa gum as well as a preparation method and application thereof, and relates to the technical field of natural product processing. Comprising the following steps: dissolving non-transparent caesalpinia spinosa gum; heating and raising the temperature, then adjusting the pH value, and then adding protease for enzymolysis; adjusting the pH value of the enzymolysis feed liquid, heating, preserving heat and deactivating enzyme; then carrying out column adsorption filtration, then carrying out fine filtration, and adjusting the pH value of a fine filtrate; and finally, concentrating to obtain a caesalpinia spinosa gum concentrated solution. The process design thought is ingenious, the operation steps are simple and convenient, the process is reasonable, the obtained product has the characteristics of being clear and transparent, the solubility and the purity are high, the purpose of maximizing the output value is achieved, the product has unique system stability and taste blending effects when applied to food, health care products and pharmaceuticals, and the product has good market prospects when applied to cosmetics. The skin care lotion has unique application values of skin nourishing and caring and skin moisturizing, and is suitable for large-scale popularization and application.

Description

technical field [0001] The invention relates to the technical field of natural product processing, in particular to a highly transparent tara gum and its preparation method and application. Background technique [0002] Tara gum, also known as tara gum, tara gum, and tara gum, is a natural product made from the shrubs of Peru, using the endosperm of the seeds of the legume family Tara gum as raw material, and processed . Tara gum has good thermal stability, chemical stability and colloidal compounding properties. It is a natural edible colloid with excellent performance. It is mainly used as a thickener, gelling agent and system stabilizer, and can be widely used in food , Health products, pharmaceuticals, cosmetics processing and production. Tara gum has good water solubility and has high viscosity characteristics at low concentrations. 1% tara gum has good solubility in cold water. At 25°C, it has a very good viscosity. At 45°C, it dissolves 100%, forming a milky white,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08B37/00A23L29/238A23L33/125A61K8/73A61K47/36A61Q19/00A61Q19/02
CPCC08B37/0087A23L29/238A23L33/125A61K47/36A61K8/73A61Q19/00A61Q19/02
Inventor 刘星丁作坤王纪文
Owner SHANGHAI HOPE TEC BIOTECH
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