Quick-dry filament, preparation method thereof and toothbrush
A quick-drying and fibril technology, applied in the field of fibrils, can solve the problems that toothbrushes are prone to bacteria breeding, and achieve the effects of reducing bacterial growth, improving waterproof performance, and not easy to break
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preparation example 1
[0073] A modified hydrophobic silica, obtained by the following method:
[0074] S1, weigh 0.4Kg of silicon dioxide, and dry it under the condition of 200°C, and the drying time is 2h to obtain a dry product;
[0075] S2. Weigh 0.1Kg of methanol and heat it to 50°C, add the dried product in S1, stir, add 0.1Kg of organosilane coupling agent, react for 30mim, add 0.2Kg of sulfuric acid solution with a mass fraction of 10%, stir for 10min, filter, Wash with propylene glycol and dry to obtain an intermediate product;
[0076] S3: Weigh 0.1 Kg of talc powder and mix with the intermediate product obtained in S2 to obtain modified hydrophobic silica, and the mixing speed is 1000 r / min.
preparation example 2
[0078] A modified hydrophobic silica, obtained by the following method:
[0079] S1, weigh 0.5Kg of silicon dioxide, and dry it under the condition of 225°C, and the drying time is 2.5h to obtain a dry product;
[0080] S2. Weigh 0.13Kg of methanol and heat it to 55°C, add the dried product in S1, stir, add 0.13Kg of organic silane coupling agent, react for 40mim, add 0.25Kg of sulfuric acid solution with a mass fraction of 18%, stir for 15min, filter, Wash with propylene glycol and dry to obtain an intermediate product;
[0081] S3: Weigh 0.15Kg of sodium stearate and mix with the intermediate product obtained in S2 to obtain modified hydrophobic silica, and the mixing speed is 1300r / min.
preparation example 3
[0083] A modified hydrophobic silica, obtained by the following method:
[0084] S1, take by weighing 0.6Kg of silica, under the condition of 250 ℃, carry out drying, drying time is 3h, obtains drying product;
[0085] S2. Weigh 0.15Kg of methanol and heat it to 55°C, add the dried product in S1, stir, add 0.13Kg of organic silane coupling agent, react for 60mim, add 0.3Kg of sulfuric acid solution with a mass fraction of 25%, stir for 20min, filter, Wash with propylene glycol and dry to obtain an intermediate product;
[0086] S3: Weigh 0.2Kg of zinc stearate and mix with the intermediate product obtained in S2 to obtain modified hydrophobic silica, and the mixing speed is 1500r / min.
[0087] The types and amounts of various components in Preparation Examples 1 to 3 are shown in Table 2:
[0088] Table 2 Types and dosages of various components in Preparation Examples 1 to 3
[0089]
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