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Method for processing and using SiC substrate without positioning edge

A processing method, a technology without positioning, applied in chemical instruments and methods, polycrystalline material growth, crystal growth and other directions, which can solve the problems of not substantially improving the positioning edge stress, reducing the utilization area of ​​the substrate, and high probability of crystal cracking. , to achieve the effect of improving production quality and yield, reducing production costs, and reducing crystal processing costs

Pending Publication Date: 2022-08-02
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] (1) During the process of grinding out the positioning edge of the crystal end face, the chance of crystal cracking is relatively high;
[0007] (2) The ground crystal is no longer a complete circle. When this type of substrate is used as the seed crystal, defects such as micropipes and stress accumulation will appear in the grown SiC single crystal, which will affect the quality of the single crystal;
[0008] (3) As the diameter of the crystal increases, in order to intuitively distinguish the main positioning edge and the secondary positioning edge, the length of the two positioning edges also needs to increase accordingly, resulting in a decrease in the available area of ​​the substrate
[0012] However, in this method, there are still two positioning edges on the SiC substrate, and the stress near the positioning edges has not been substantially improved.

Method used

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  • Method for processing and using SiC substrate without positioning edge
  • Method for processing and using SiC substrate without positioning edge
  • Method for processing and using SiC substrate without positioning edge

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Embodiment approach

[0054] Embodiments of the invention and features of the embodiments may be combined with each other without conflict.

[0055] Terminology Description:

[0056] Seed face: refers to the side of the crystal that contains the seed;

[0057] Primary surface: refers to the growth surface of the crystal. Generally, the surface is uneven, and there are growth stripes, facets, etc.;

[0058] Cutting head piece: refers to the first cutting piece near or / and containing the seed crystal, generally there is a carbon ring around it;

[0059] Cutting tail piece: refers to the first cutting piece close to or / and including the natural surface, generally the diameter is smaller than the target diameter, and there is a "slope";

[0060] Off-axis SiC crystal: It means that the surface normal of the crystal does not coincide with the c-axis, and deviates from the c-axis by a certain small angle along the [11-20] or [1-100] direction.

[0061] According to the prior art, the presence of V-shap...

Embodiment 1

[0063] attached figure 1 As shown, this embodiment discloses a method for processing and using a SiC substrate without positioning edges, including:

[0064] 1) Spheronization: The grown SiC crystal is subjected to cylindrical grinding to make the outer diameter of the SiC crystal to the target size;

[0065] 2) Orientation: use the orientation instrument to orient the outer circle of the crystal, accurately determine the [1-100] and [11-20] directions of the crystal, and mark the outer circle of the crystal;

[0066] 3) Crystal cutting: The crystal is bonded to the cutting base according to a specific direction, and the cutting process parameters are set by a multi-wire cutting machine, and the SiC crystal is processed into a cutting piece;

[0067] 4) Cut and take slices: use a heating platform to bake the slices from the cutting base, take out and mark the carbon silicon surface of the head or tail of the slice, and clean the slice to remove the residual cutting fluid on t...

Embodiment 2

[0090] The purpose of this embodiment is to provide a 4H-SiC substrate processing and using method without positioning edges, which specifically includes the following operation steps:

[0091] 1) Spheronization: The silicon surface obtained by the growth is subjected to cylindrical grinding along the [11-20] direction off-axis to the 4°SiC crystal, so that the outer diameter of the 4H-SiC crystal is processed to 150mm;

[0092] 2) Orientation: Use the orientation instrument to orient the outer circle of the crystal, accurately determine the and [11-20] directions of the crystal, and mark the crystal orientation with a marker on the outer circle of the crystal. The crystal plane and the original plane are marked with silicon plane and carbon plane respectively;

[0093] 3) Crystal cutting: The [11-20] direction of the crystal mark is vertically upward, and then the crystal is bonded to the graphite cutting base, and the cutting process parameters are set by a multi-wire cutti...

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Abstract

The invention provides a method for processing a SiC substrate without a positioning edge. The method comprises the following steps: orienting the excircle of a SiC crystal; crystal cutting; the cutting blade is baked from the cutting base and taken out, the carbon-silicon surface of the head blade or the tail blade of the cutting blade is marked, and the cutting blade is cleaned to remove residual cutting fluid on the surface; orienting head and tail pieces: orienting the head and tail cutting pieces of the SiC crystal, and verifying the [1-100] and [11-20] directions of the head piece or the tail piece of the marked cutting piece; orientation of non-head and non-tail wafers: overlapping the non-head and non-tail wafers with the head wafer and / or the tail wafer to enable the tool marks of the non-head and non-tail wafers to coincide, then performing orientation along the off-axis direction of the wafer, and determining the off-axis direction and the polar surface of the wafer; carbon / silicon surface marking and crystal orientation marking; and carrying out subsequent process treatment on the marked wafer to obtain the SiC substrate without the positioning edge. When the positioning-edge-free SiC substrate prepared in the invention is used as a seed crystal or a substrate for growing a SiC crystal or an epitaxial wafer, the defects of microtubules, stress and the like in the crystal can be effectively reduced, and the quality of the material is greatly improved.

Description

technical field [0001] The invention belongs to the technical field of single crystal processing, and in particular relates to a processing and using method of a SiC substrate without positioning edges. Background technique [0002] The statements in this section merely provide background information related to the present invention and do not necessarily constitute prior art. [0003] Silicon carbide (SiC) is a relatively mature third-generation semiconductor material. It has excellent semiconductor properties such as high temperature resistance, high thermal conductivity, and high breakdown voltage, enabling SiC-based devices to work under extreme conditions. At the same time, SiC, as an important substrate material, can be used for epitaxial growth of gallium nitride, graphene, etc. At present, β-SiC substrates such as 4H-SiC and 6H-SiC are widely used in high-power power electronic devices, microwave radio frequency devices and optoelectronic devices. [0004] SiC is a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01L21/02C30B23/02C30B25/18C30B29/36
CPCC30B23/025C30B25/18C30B29/36H01L21/0201H01L21/02027H01L21/02013
Inventor 谢雪健徐现刚陈秀芳胡小波
Owner SHANDONG UNIV
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