Solidifing agent of modified like epoxy resins by alcyl amine
An epoxy resin curing and epoxy resin technology, which is applied in the field of alicyclic amine modified epoxy resin curing agent and its preparation, can solve the problems of irritating volatiles, polluting the environment, moisture absorption and whitening, etc. The effect of fast curing speed, light color and correct operation method
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[0015] Specific embodiments of the present invention will be described in detail below.
[0016] Add 100 mol of aminomethylcyclopentylamine and 100±10 mol of butyl glycidyl ether in the installed enamel glass reaction kettle, metering tank, vacuum pump, dry nitrogen protection and other devices at room temperature; replace the air in the reaction kettle with nitrogen , start stirring and raise the temperature to 50°C at the same time, control the temperature at 50-90°C, and control the reaction temperature by passing cooling water during the feeding process. Maintain 90°C for 90 minutes, cool down to 35°C and pack. Dry nitrogen filled the remainder of the autoclave throughout the reaction.
[0017] According to above-mentioned method and formula, the performance that obtains product is as follows:
[0018] Appearance Colorless or light yellow flowing liquid
[0019] Viscosity 10~25s (coat 4 cups)
[0020] Amine equivalent 100~130g / mol
[0021] Active hydrogen equivalent 8...
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