Process for extraction refining amygdalin
The technology of amygdalin and purpose is applied in the field of separation and purification of extracting amygdalin, which can solve the problems of flammability and explosion, high solvent, and low product purity, and achieves no fire danger, mild operating conditions, and no environmental pollution. Effect
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example 1
[0021] Take the seeds of Plum, crush them into 10-40 meshes, weigh 200 grams of raw materials, put them in an extractor and pass them through supercritical CO 2 Deoiling after fluid extraction, extraction pressure 30MPa, extraction temperature 40°C, separation pressure 8MPa, separation temperature 50°C, after 4 hours, discharge the slag powder from the bottom of the extractor, add 1200ml of ethanol, and extract three times, each time 400 ml, combined the filtrates, recovered ethanol to an appropriate amount under reduced pressure, and vacuum-dried at 65° C. for 3 hours to obtain 11 g of a brownish-yellow extract, the content of which was determined to be 55% by HPLC.
[0022] Take 3 grams of the extracted extract, add a small amount of ethanol to dissolve and filter, then place it in a refrigerator at 4°C for 10 hours, and white crystals precipitate, filter, wash with a small amount of ethanol, and dry to obtain 1.3 grams. After HPLC detection, the content reaches 98.0% .
example 2
[0024] Take the seeds of Prunus mellifera, grind them into 20-40 mesh with a shear pulverizer, weigh 200 grams of raw materials, and put them in an extractor through supercritical CO 2 Deoiling after fluid extraction, extraction pressure 20MPa, extraction temperature 60°C, separation pressure 9MPa, separation temperature 70°C, after 6 hours, discharge the slag powder from the bottom of the extractor, add 1200ml of ethanol, and extract three times, each time 400 ml, combined the filtrates, recovered ethanol to an appropriate amount under reduced pressure, and dried in vacuo at 65°C for 3 hours to obtain 12 g of a brownish-yellow extract, the content of which was determined by HPLC to be 50%.
[0025] 4 g of the extracted extract was dissolved by adding a small amount of ethanol sonicated, then stood still at room temperature for 1 hour, filtered to obtain white crystals, and dried to obtain 1.6 g. The content reached 92.3% through HPLC detection.
example 3
[0027] Take the seeds of bitter almonds, grind them into 20-40 meshes with a shearing mill, weigh 200 grams of raw materials, and put them in an extractor through supercritical CO 2 Deoiling after fluid extraction, extraction pressure 32MPa, extraction temperature 50°C, separation pressure 5Mpa, separation temperature 30°C, after 4 hours, discharge the slag powder from the bottom of the extractor, add 1500ml of ethanol, and extract three times, each time 500 ml, combined the filtrates, recovered ethanol to an appropriate amount under reduced pressure, and vacuum-dried at 65° C. for 3 hours to obtain 5.5 g of brown-yellow extract, the content of which was 60% as determined by HPLC.
[0028] Take 4 grams of the extracted extract, add a small amount of ethanol to dissolve and filter, then place it at 4 ° C for 10 hours, precipitate white crystals, filter, wash with a small amount of ethanol, and dry to obtain 1.8 grams. After HPLC detection, the content reaches 95.4%.
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