35results about How to "Low extraction efficiency" patented technology

The invention relates to a production method of 2,3-dichloropyridine, solving the problem that byproducts are easily generated through 2-position chlorination reaction so as to cause the final product quality to be instable, for example, intermediate purification is carried out but yield and environment are influenced, and the working efficiency is reduced. The production method of the 2,3-dichloropyridine comprises the following steps: 1) carrying out degradation reaction: hydrolyzing 2-chloro nicotinamide used as a starting material, and carrying out solid-liquid separation to obtain 2-chlorine-3-aminopyridine; and (2) successively carrying out diazotization reaction and 3-position chlorination reaction: successively carrying out diazotization reaction and 3-position chlorination reaction on 2-chlorine-3-aminopyridine to obtain 2,3-dichloropyridine. The production method has the beneficial effects that (1) the difficulty that the byproducts are easily generated because 2-position chlorination is successfully avoided, thereby ensuring the quality of the intermediate product 2-chlorine-3-aminopyridine; and (2) because the intermediate product 2-chlorine-3-aminopyridine is not dissolved in strong basic aqueous solution, the product can be directly taken out by vacuum filtration, and is easy to purify.

The invention provides a liquid chromatography-mass spectrometry method for rapidly detecting the content of beta-agonists. The liquid chromatography-mass spectrometry method comprises the following steps: pretreating a sample, namely, sequentially adding water and an organic extracting solution in the sample for extracting a beta-receptor stimulant; then adding a salting-out agent and a water removing agent to ensure that the organic extracting solution and a water phase demix, centrifuging to obtain a first supernate, adding an adsorbing agent in the first supernate for purification, centrifuging to obtain a second supernate, concentrating, re-dissolving and filtering the second supernate to prepare a sample to be detected; and then detecting the beta-receptor stimulant contained in an animal-derived food by adopting an ultra-high performance liquid chromatography-triple quadrupole mass spectrometer. According to the sample pretreatment method suitable for liquid chromatography-mass spectrometry detection, provided by the invention, interfering molecules are removed through extraction and purification so that high accuracy is achieved in sample detection.

The invention discloses a method for continuous fractional separation and purification of effective ingredients of star anise, and relates to purification of a natural product of star anise. The invention provides a method for continuous fractional separation and purification of the effective ingredients of the star anise, which can ensure the extraction efficiency of a target product, has low production operating cost, high solvent recovery rate and obviously low energy consumption, and is suitable for large-scale production. The method comprises the following steps of: extracting star aniseoil; extracting star anise oil resin; separating anethole from anisaldehyde; performing microbial conversion on shikimic acid; and extracting and separating the shikimic acid. On the basis of extracting the star anise oil resin and separating the anethole from the anisaldehyde, the shikimic acid is extracted and separated from extraction residue, products with high added value, such as shikimi fruit, the anethole and the anisaldehyde are obtained, and the extraction efficiency of the target product is ensured.

The invention provides a process for extraction refining amygdalin which consists of, disintegrating the plant raw material containing rich bitter apricot seed into powder, removing the grease from the raw material powder by using CO2 as extracting agent, carrying out decompression segregation to the carbon dioxide containing vegetable fat, charging alcohol into ground-slag containing bitter apricot seed glycosides by the solid-to-liquid ratio of 1 : 3-10, agitating, filtering by suction to obtain the filter liquor, distilling and drying the filter liquor to obtain crude product of bitter apricot seed glycoside, dissolving the bitter apricot seed glycoside into ethanol, low temperature crystallizing, filtering and drying to obtain the high purity bitter apricot seed glycosides.

The invention discloses a display panel, a manufacturing method thereof and a display device, wherein the display panel is divided into a display area and a non-display area surrounding the display area, the display area includes an edge area and a non-edge area, and the edge area of ​​the display area and the non-display area The regions are connected and surround the non-edge area; the display panel includes a light extraction layer, and the thickness of the light extraction layer in the edge area of ​​the display area is greater than that in the non-edge area of ​​the display area, which can make the light extraction efficiency in the edge area of ​​the display area higher. In the non-edge area of ​​the display area, the light extraction efficiency is relatively low, and the light output in the edge area of ​​the display area is enhanced by increasing the thickness of the light extraction layer in the edge area of ​​the display area, so that the brightness of the edge area increases, and then the non-edge area is reduced. The brightness difference between the edge area and the edge area makes the brightness of the edge area of ​​the display panel tend to be consistent with the brightness of the non-edge area, which improves the display uniformity of the display panel, thereby improving the display effect.

The invention discloses a method for recovering sulfur, lead, zinc and silver from oxygen-rich direct leaching residues of zinc concentrate or lead and zinc mixed ores by virtue of ultrasonic wave intensification, belonging to the field of comprehensive recycling of non-ferrous metal metallurgy. The method disclosed by the invention comprises the following steps: by using tetrachloroethylene or trichloro ethylene as a solvent, extracting elemental sulfur from the oxygen-rich direct leaching residues of zinc concentrate or lead and zinc mixed ores, which are dried, ground, and sieved by virtue of ultrasonic wave intensification, preserving heat and filtering, after naturally cooling and forcibly cooling the filtrate and filtering to obtain a sulfur product, and returning a regenerated sulfur extraction agent to a sulfur extraction step; and enriching zinc, lead and silver in the residues, wherein the residues can be directly fed to a lead system to recover zinc, lead and silver, or the residues are firstly leached to recover zinc, filter residues are fed to the lead system to recover silver, and zinc-containing filtrate is returned to a direct leaching system. The method disclosed by the invention is simple, energy-saving and high in sulfur recovery rate and product quality. The sulfur extraction process is sealed, so that the method is free from environmental pollution and is particularly suitable for comprehensively utilizing normal pressure / high pressure oxygen-rich direct leaching residues of zinc concentrate or lead and zinc mixed ores.