Self toughening silion nitride ceramic guide and guard roller and its preparing method
A technology of toughened silicon nitride and guide rollers, which is applied in the field of self-toughened silicon nitride ceramic guide rollers and its preparation, which can solve the problems of frequent replacement, failure of guide rollers due to high-temperature wear, and material consumption of guide rollers.
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Embodiment 1
[0023] 1) Preparation of β-Si 3 N 4 Seed crystal: Add 100 grams of ytterbium oxide to 900 grams of α-phase silicon nitride powder fine powder, put the powder into a stirring mill, use silicon nitride balls as the ball milling medium, and absolute ethanol as the mixing medium, powder, The mass ratio of grinding balls and ethanol is 1:1.5:2. After ball milling for 24 hours, dry in a double-cone rotary vacuum dryer. Put the powder into a graphite crucible, heat at 1550°C for 3 hours in a nitrogen atmosphere, grind the powder, and pass through a 200-mesh sieve to obtain β-Si 3 N 4 Seed.
[0024] 2) Mixing: Add 300 grams of ytterbium oxide and 100 grams of prefabricated β-Si to 600 grams of raw material α-phase silicon nitride fine powder 3 N 4 Seed. Put the powder into a stirring mill, use silicon nitride balls as the ball milling medium, acetone as the mixing medium, and the mass ratio of powder, balls and acetone is 1:1.5:2. After ball milling for 12 hours, dry in a doub...
Embodiment 2
[0030] 1) Preparation of β-Si 3 N 4 Seed crystal: Add 150 grams of ytterbium oxide to 850 grams of α-phase silicon nitride powder fine powder, put the powder into a stirring mill, use silicon nitride balls as the ball milling medium, and acetone as the mixing medium, powder, milling balls The mass ratio to ethanol is 1:1.5:2. After ball milling for 24 hours, dry in a double-cone rotary vacuum dryer. Put the powder into a graphite crucible, heat at 1650°C for 1 hour in a nitrogen atmosphere, grind the powder, and pass through a 200-mesh sieve to obtain β-Si 3 N 4 Seed.
[0031] 2) Mixing: Add 200 grams of ytterbium oxide and 80 grams of prefabricated β-Si to 720 grams of raw material α-phase silicon nitride fine powder 3 N 4 Seed. Put the powder into a stirring mill, use silicon nitride balls as the ball milling medium, acetone as the mixing medium, and the mass ratio of powder, balls and ethanol is 1:1.5:2. After ball milling for 24 hours, dry in a double-cone rotary v...
Embodiment 3
[0037] 1) Preparation of β-Si 3 N 4Seed crystal: Add 150 grams of ytterbium oxide to 850 grams of α-phase silicon nitride powder fine powder, put the powder into a stirring mill, use silicon nitride balls as the ball milling medium, and absolute ethanol as the mixing medium, powder, The mass ratio of grinding balls and ethanol is 1:1.5:2. After ball milling for 24 hours, dry in a double-cone rotary vacuum dryer. Put the powder into a graphite crucible, heat at 1750°C for 0.5 hours in a nitrogen atmosphere, grind the powder, and pass through a 200-mesh sieve to obtain β-Si 3 N 4 Seed.
[0038] 2) Mixing: Add 100 grams of ytterbium oxide and 50 grams of prefabricated β-Si to 850 grams of raw material α-phase silicon nitride fine powder 3 N 4 Seed. Put the powder into a stirring mill, use silicon nitride balls as the ball milling medium, absolute ethanol as the mixed medium, and the mass ratio of the powder, the balls and the ethanol is 1:1.5:2. After ball milling for 40 ...
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