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Carbon oil in use for making carbon resistance element, preparation method, and prepared element of carbon resistance

A carbon oil and component technology, applied in the manufacturing of electrical components, resistors, resistors, etc., can solve the problems of cumbersome process, cumbersome preparation process, destroying the performance of carbon resistance components and product resistance stability.

Inactive Publication Date: 2006-07-05
BYD CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example, it is necessary to prepare carbon oil with a square resistance of 300 ohm / square / 25μm±10%, then choose carbon oil with a square resistance of 400 ohm / square / 25μm±10% as the main component, and use it to combine with the square resistance The carbon oil product of 40 ohms / square / 25μm±10% is mixed in a certain proportion to prepare the carbon oil with the required square resistance value. On the one hand, it is necessary to conduct additional experiments to determine the ratio of the two carbon oils. The process is relatively On the other hand, due to the uniformity of mixing, the resistance range of carbon oil after mixing becomes wider, for example, from the original ±10% to ±20% or wider. In addition, the air bubbles introduced during the mixing process will be in the Defects such as pinholes and cracks are formed in the final carbon resistance element, thereby destroying the performance of the product and the stability of the product resistance value
That is to say, the problems existing in the prior art are: the preparation process is relatively cumbersome, the resistance value distribution range of the formed carbon resistance element is wide due to the uniformity of mixing, and the air bubbles introduced during the mixing process will introduce needles into the final product. Defects such as holes and cracks will destroy the performance of carbon resistance components and the stability of product resistance

Method used

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  • Carbon oil in use for making carbon resistance element, preparation method, and prepared element of carbon resistance
  • Carbon oil in use for making carbon resistance element, preparation method, and prepared element of carbon resistance
  • Carbon oil in use for making carbon resistance element, preparation method, and prepared element of carbon resistance

Examples

Experimental program
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Effect test

Embodiment 1

[0047] according to figure 1 As shown in the process flow chart of preparing carbon resistance element, weigh the conductive carbon black (V-XC605, the average particle size is 35nm, the DBP value is 148cc / 100g, the BET surface area is 90m 2 / g) and nickel powder (INCO110, spherical particles, average particle size 0.8-1.5μm, BET surface area 0.9-2.0m 2 / g, volume resistivity 1.18μΩ·cm) 50 parts by weight of two conductive fillers (the weight ratio of the two is 3:1), dried in vacuum, mixed by a ball mill, and added 4% of the carbon black weight compound type A toluene solution of monoalkoxy titanate coupling agent (CT-136) (the concentration of the solution is 10 wt%) was mixed on a high-speed mixer for 2 hours, and then the solvent was evaporated. The resulting mixture was added to 100 parts by weight of polyvinyl butyral (Butvar  B-76) and 500 parts by weight of methyl ethyl ketone and mixed uniformly, and then 100 parts by weight of phenolic resin (Santolink  EP560) methyl ...

Embodiment 2

[0050] Weigh Conductex SC Ultra carbon black (average particle size is 20nm, DBP value is 115cc / 100g, BET surface area is 205m 2 / g) and nickel powder (INCO210, chain bead powder, average particle size 0.5-1.0μm, BET surface area 0.9-2.0m 2 / g, volume resistivity 1.18μΩ·cm) 100 parts by weight of the two conductive fillers (the weight ratio between the two is 4:1), dried in vacuum, mixed by a ball mill, and added 4% by weight of silane coupling agent ( DOWCORNING  Z-6032) Mix on a high-speed mixer at 80°C for 2 hours. The resulting mixture was added to a solution consisting of 100 parts by weight of polyester polyurethane (product of Luoyang Liming Chemical Research Institute) and 800 parts by weight of ethanol and mixed uniformly, and then 100 parts by weight of a mass percentage concentration of 5 % Epoxy resin (Araldite TM 6069) After mixing the solution uniformly, the carbon oil product of the present invention is prepared.

[0051] Using the above carbon oil, manually screen...

Embodiment 3

[0053] Weigh Conductex SC Ultra carbon black (average particle size is 20nm, DBP value is 115cc / 100g, BET surface area is 205m 2 / g) and silver powder (ECP-Ag-F1, flakes, average particle size of 2-4μm, volume resistivity 1.6μΩ·cm) two conductive fillers 80 parts by weight (the weight ratio of the two is 5:1) , Vacuum drying, after mixing through a ball mill, add 5 wt% silane coupling agent (DOWCORNING  Z-6106), mixed on a high-speed mixer at 60°C for 2 hours. The resulting mixture was added to 100 parts by weight of polyvinyl butyral (Butvar  B-76) and 600 parts by weight of ethyl acetate and mixed uniformly, and then 100 parts by weight of 5% by mass melamine resin (Resimene 717) After mixing the solution uniformly, the carbon oil product of the present invention is prepared.

[0054] Using the above carbon oil, manually screen printing on the rigid circuit board, such as figure 2 The resistance of the carbon resistance element shown was tested after curing at 150°C for 30 m...

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Abstract

The carbon oil is composed of current conducting padding, rosin joint material, cross-linking agent, and solvent. The padding includes carbon black, metal powder or mixture of powder of electroconductive metallic compound. The said metal powders can be powders of nickel, silver, gold, aluminum, zinc, tin or stainless steel. Mixture of powder can be nickel oxide, tin oxide, indium oxide, niobium oxide or iron phosphide. Features are: simple technique, narrow distribution range of numerical value of resistance in mean square. The invention overcomes defects of pinholes, cracks etc. in final product so as to raise capability of product and stability of carbon resistance element.

Description

Technical field [0001] The invention belongs to the technical field of resistors, and relates to a carbon oil used for making a carbon resistance element, a preparation method thereof, and a carbon resistance element made by using the carbon oil. Background technique [0002] The traditional preparation method of carbon resistance element includes: dispersing a certain amount of conductive carbon black in a thermosetting resin solution to prepare a paste, namely carbon oil, and then applying the carbon oil to FR1, FR2, FR4, etc. by screen printing. The surface of the rigid printed circuit board substrate is formed with a pattern of a certain shape and size, and finally heated to evaporate the solvent and further heated to 100-180°C to cure the resin, thereby forming a carbon resistance element. [0003] Generally speaking, as the content of carbon black in the carbon oil increases, the conductivity of the system increases and the resistance value decreases, but the resistance cha...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01B1/20H01C7/00H01C17/065
Inventor 章颂云
Owner BYD CO LTD
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