Method for processing cobalt copper alloy
A cobalt-copper alloy and process technology, which is applied in the field of cobalt-copper alloy treatment by wet method, can solve the problems affecting the recovery rate of cobalt and copper, the leaching process efficiency is not high, and the reaction speed is slow, so as to achieve high leaching operation efficiency and easy control , fast response effect
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Embodiment 1
[0029] Example 1 Take 1000 grams of cobalt-copper alloy and put it into a ball mill for 90 minutes, and then vibrate mill it for 120 minutes. The average particle size is 47 microns. Take by weighing 80 grams of this alloy, 80 grams of ammonium chloride, 20 grams of ferric chloride, 133 milliliters of 36% hydrochloric acid, add 500 milliliters of water, heat up to 87 degrees, feed air (flow rate is 1.2 liters / minute), under stirring condition The reaction was carried out for 8 hours, and the pH at the end of the reaction was 3.5. Then the slurry is magnetically separated and filtered. 2.6 grams of unreacted residual cobalt-copper alloy were magnetically separated, and the obtained leaching solution contained 26.9 grams / liter of cobalt, 24.8 grams / liter of copper, and 0.06 grams / liter of iron. The leaching slag contains 0.42 grams of cobalt and 0.30 grams of copper. The leaching rate of cobalt was 94.3%, and the leaching rate of copper was 95.2%. The actual yield of cobalt w...
Embodiment 2
[0030] Example 2 Take 1000 grams of cobalt-copper alloy and put it into a ball mill for 90 minutes, and then vibrate mill it for 120 minutes. The average particle size is 47 microns. Weigh 80 grams of the alloy, 50 grams of ammonium chloride, 30 grams of sodium fluoride, 133 milliliters of 36% hydrochloric acid, add 500 milliliters of water, heat up to 87 degrees, feed air (flow rate is 1.2 liters / min), and stir The reaction was carried out for 8 hours, and the pH value at the end of the reaction was 3.5. Then the slurry is magnetically separated and filtered. 2.1 grams of unreacted residual cobalt-copper alloy were magnetically separated, and the obtained leaching solution contained 32.8 grams / liter of cobalt, 27.6 grams / liter of copper, and 0.08 grams / liter of iron. The leaching slag contains 0.31 grams of cobalt and 0.33 grams of copper. The leaching rate of cobalt was 95.8%, and the leaching rate of copper was 95.5%. The actual yield of cobalt was 98.4%, and that of cop...
Embodiment 3
[0031]Example 3 Take 1000 grams of cobalt-copper alloy and put it into a ball mill for 90 minutes, and then vibrate mill it for 120 minutes. The average particle size is 47 microns. Weigh 160 grams of this alloy, 50 grams of ammonium chloride, 30 grams of sodium fluoride, 20 grams of ferric chloride, 266 milliliters of 36% hydrochloric acid, add 500 milliliters of water, heat up to 87 degrees, feed air (flow rate is 1.5 liters / After 6.5 hours of reaction under stirring conditions, slowly add 5% sodium hydroxide solution until the pH value is 4.0, and continue the reaction for 45 minutes. Then the slurry is magnetically separated and filtered. 3.5 grams of unreacted residual cobalt-copper alloy were magnetically separated, and the obtained leaching solution contained 57.2 grams / liter of cobalt, 50.0 grams / liter of copper, and 0.005 grams / liter of iron. The leaching slag contains 0.39 grams of cobalt and 0.77 grams of copper. The leaching rate of cobalt was 96.6%, and the lea...
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