Laminate of magnetic base material and method for production thereof
A technology of magnetic substrates and manufacturing methods, applied in the direction of magnetic materials, magnetic objects, and the magnetism of inorganic materials, can solve problems such as retention, lower rated power, and disadvantages, and achieve high duty cycle, high thermal conductivity, and temperature rise low effect
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Embodiment 1
[0050] As the magnetic thin metal plate, Metglas: 2605TCA (trade name) manufactured by Hanewell Co., Ltd. was used. 78 B 13 Si 9 (atomic %) thin strips of amorphous metal. Use a roll coater to coat a polyamic acid solution with a viscosity of about 0.3 Pa·s at 25°C measured by an E-type viscometer on the entire surface of one side of an amorphous metal strip, dry it at 140°C, and then dry it at 260°C. It is solidified at ℃, and a heat-resistant resin (polyimide resin) of about 4 microns is formed on one side of the amorphous metal strip. Polyimide resin is mixed with 3,3'-diaminodiphenyl ether and 3,3',4,4'-biphenyltetracarboxylic dianhydride in the ratio of 1:0.98, in dimethylacetamide solvent A resin obtained by polycondensation at room temperature. Usually, polyamic acid is used as a diacetamide solution.
[0051] In addition, the resin-coated magnetic base material was cut into 50 mm squares, 50 sheets were stacked, and laminated under pressure at 270° C. and 10 MPa f...
Embodiment 2
[0056] As the magnetic thin metal plate, Metglas: 2714A (trade name) manufactured by Hanewell Co., Ltd. with a width of about 50 mm and a thickness of about 15 μm is used. 66 Fe 4 Ni 1 (BSi) 29 (atomic %) thin strips of amorphous metal. Use a roll coater to coat the polyamic acid solution with a viscosity of about 0.3 Pa·s at 25°C when measured by an E-type viscometer on the entire surface of one side of the thin strip, dry it at 140°C, and heat it at 260°C. Curing at the bottom to give a heat-resistant resin (polyimide resin) of about 4 microns on one side of the amorphous metal strip. Polyimide resin is mixed with 3,3'-diaminodiphenyl ether and 3,3',4,4'-biphenyltetracarboxylic dianhydride in the ratio of 1:0.98, in dimethylacetamide solvent obtained by polycondensation at room temperature. Usually, polyamic acid is used as a diethylamide solution.
[0057] In addition, the resin-coated magnetic base material was cut into 30 mm squares, and 50 pieces were stacked, and ...
Embodiment 3
[0061] As the magnetic metal thin plate, a nanocrystalline magnetic metal ribbon having a composition of Fe, Cu, Nb, Si, and B elements, Fe, Cu, Nb, Si, and B, was used as Fe, Cu, Nb, Si, and B elemental Fe, Cu, Nb, Si, and B. Coat the same resin as in Example 1 to make a magnetic substrate, cut it into a square of 30 mm, overlap 50 pieces, pressurize for 30 minutes at 270 ° C and 10 MPa in a nitrogen atmosphere, and then laminate and integrate it. Heat treatment at 550°C and 1Mpa for 1.5 hours. Then, for evaluation, the space factor and the volume resistivity prescribed by JIS H 0505 were measured. In addition, the thermal conductivity specified in JIS R 1611 was measured.
[0062]In order to measure the temperature rise when an alternating magnetic field is applied, the magnetic base material of this example is punched into a ring shape with an outer diameter of 40mm and an inner diameter of 25mm with a metal mold. Next, pressurize with a hot press for 30 minutes to carry ...
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