Method for preparing ultra-fine crystal WC-Co hard alloy
A cemented carbide and ultra-fine grain technology, which is applied in the field of high-performance functional materials to achieve the effects of high hardness, small grain size and broad application prospects.
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[0016] Example 1:
[0017] Raw materials: the mass ratio of WC powder with a particle size of 0.2 μm, pure Co powder and VC powder with a particle size of 2.94 μm is 88.7:11:0.3.
[0018] Take the raw material powder of the above ratio and mix it evenly by high-energy ball milling for 30 minutes. After drying, it is put into a graphite mold for hot pressing and sintering. The sintering process is: heating at a heating rate of 50°C / min, applying a pressure of 40MPa, and when the temperature When the temperature is raised to 750°C, the temperature is kept for 5 minutes, and the hot pressing is completed. When it is cooled to below 100°C, take it out and demould. Then combine the hot-pressed compact, graphite sealing sheet, carbon steel pressurized sheet, and pyrophyllite sheath that integrates insulation, heat insulation and pressure transmission. The combined sample is placed in a six-sided top press for super Electric sintering under high pressure, the sintering voltage is 1.25V, ...
Example Embodiment
[0019] Example 2:
[0020] Raw materials: WC powder with a particle size of 0.2μm, pure Co powder and Cr with a particle size of 3.6μm 3 C 2 The powder mass ratio is 88.6:11:0.4.
[0021] Take the raw material powder of the above ratio and mix it evenly by high-energy ball milling for 30 minutes. After drying, it is put into a graphite mold for hot pressing and sintering. The sintering process is: heating at a heating rate of 50°C / min, applying a pressure of 40MPa, and when the temperature When the temperature is raised to 750°C, the temperature is kept for 5 minutes, and the hot pressing is completed. When it is cooled to below 100°C, take it out and demould. Then combine the hot-pressed compact, graphite sealing sheet, carbon steel pressurized sheet, and pyrophyllite sheath that integrates insulation, heat insulation and pressure transmission. The combined sample is placed in a six-sided top press for super Electric sintering under high pressure, the sintering voltage is 1.25V, ...
Example Embodiment
[0022] Example 3:
[0023] Raw materials: WC powder with a particle size of 0.5μm, pure Co powder and Cr with a particle size of 3.6μm 3 C 2 The powder mass ratio is 91.6:8:0.6.
[0024] Take the raw material powder of the above ratio and mix it evenly by high-energy ball milling for 30 minutes. After drying, it is put into a graphite mold for hot pressing and sintering. The sintering process is: heating at a heating rate of 50°C / min, applying a pressure of 40MPa, and when the temperature When the temperature is raised to 750°C, the temperature is kept for 5 minutes, and the hot pressing is completed. When it is cooled to below 100°C, take it out and demould. Then combine the hot-pressed compact, graphite sealing sheet, carbon steel pressurized sheet, and pyrophyllite sheath that integrates insulation, heat insulation and pressure transmission. The combined sample is placed in a six-sided top press for super Electric sintering under high pressure, the sintering voltage is 1.4V, th...
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