Three-segment type block releasing technique for oil layer
A three-stage, plugging-removing technology, which is applied in the direction of production fluid, wellbore/well components, drilling composition, etc., can solve the problems of oil-water well reservoir clogging, unsatisfactory effect, short validity period, etc., to slow down clogging , restore or increase permeability, and reduce energy consumption
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Embodiment 1
[0046] Formula 1: The first stage of strong penetration swelling liquid: 1% hydrogen peroxide + 0.2% 6501 + 0.05% chloroform + 0.2% sodium di-sec-octyl maleate + 98.55% water;
[0047] The second stage of acid erosion chelating liquid: 3% hydrochloric acid + 1% acetic acid + 0.5% propynol + 1.5% ammonium chloride + 0.5% hydrofluoric acid + 0.2% 6501 + 0.05% ethylenediaminetetraacetic acid (EDTA)+ 93.25% water;
[0048] The third stage squeeze protection solution: 0.6% diddecadimethylammonium bromide quaternized polymer solution + 99.4% water.
[0049] The results of the permeability recovery experiment of the artificial core plugged by polymer are shown in Table 1:
[0050] Table 1 Core permeability and recovery rate table
[0051]
Core number
K 1
(×10 -3 μm 2 )
K 2
(×10 -3 μm 2 )
K 3
(×10 -3 μm 2 )
Recovery permeability
(%)
Increase penetration
K 3 / K 2
2-1
56
12
49
87.5
4.08
2-2
54
10.9
41
76
3.76
2-3
55
11.2
46
83.6
4.1
[0052]...
Embodiment 2
[0059] Formulation 2: The first stage of strong penetration swelling liquid: 1% sodium perborate + 0.2% 6501 + 0.05% chloroform + 0.2% sodium di-secondary octyl sulfonate maleate + 98.55% water;
[0060] The second stage of acid erosion chelating liquid: 3% hydrochloric acid + 1% acetic acid + 0.5% propynol + 1.5% ammonium chloride + 0.5% hydrofluoric acid + 0.2% 6501 + 0.05% ethylenediaminetetraacetic acid (EDTA)+ 93.25% water;
[0061] The third stage squeeze protection solution: 0.6% diddecadimethylammonium bromide quaternized polymer solution + 99.4% water.
[0062] Table 3 shows the results of the permeability recovery experiment of the polymer plugged artificial core.
[0063] Table 3 Core permeability and recovery rate table
[0064]
Core number
K 1
(×10 -3 μm 2 )
K 2
(×10 -3 μm 2 )
K 3
(×10 -3 μm 2 )
Recovery permeability
(%)
Increase penetration
K 3 / K 2
[0065] 3-1
66
10.5
58.4
88.5
4.08
3-2
64
9.8
51.3
80.2
3.76
[0066] Se...
Embodiment 3
[0070] Formula 3: The first stage of strong penetration swelling liquid: 1% hydrogen peroxide + 0.2% 6501 + 0.05% chloroform + 0.2% sodium di-sec-octyl sulfonate + 98.55% water;
[0071] The second stage of acid erosion chelating solution: 10% hydrochloric acid + 1% acetic acid + 0.5% propynol + 1.5% ammonium chloride + 4% hydrofluoric acid + 0.2% 6501 + 0.05% ethylenediaminetetraacetic acid (EDTA)+ 82.75% water;
[0072] The third stage squeeze protection solution: 0.6% diddecadimethylammonium bromide quaternized polymer solution + 99.4% water.
[0073] The results of the permeability change experiment before and after the treatment of the Hailar low permeability core are shown in Table 5.
[0074] Table 5 Permeability changes before and after treatment
[0075] Core Number
[0076] It can be seen from the above table that the patented technology can effectively improve the permeability of the low-permeability Hailar oil field, that is, the patent is also applicable to low-permeabi...
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