Cold water dispersion type xanthophyll micro-capsule and its preparing method
A technology of lutein and microcapsules, applied in the field of preparation of the microcapsules, can solve the problems of high difficulty in spray drying operation, difficult to ensure uniform colloid, difficult control and operation, etc., and achieves good water solubility, low production cost, and easy operation. effect of operation
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Embodiment 1
[0033] Mix 100 grams of lutein powder, 360 grams of modified starch, 1440 grams of gelatin, and 100 grams of OP-10, add water 12 times the total weight of the above mixture, stir at 60°C for 5 hours, and control the speed at 500 rpm , after cooling, the solution is filtered, and the filtrate is sprayed and dried under the conditions of a spray dryer pressure of 8Mpa, an inlet temperature of 170°C, and an outlet temperature of 80°C to obtain an average particle size of 70 μm cold water-dispersible lutein microcapsule powder.
[0034] Following is the stability test data of the sample that embodiment 1 obtains:
[0035] Test time
(moon)
Exterior
Cold water dispersible lutein content (%)
0±2℃
25±2℃
0
Orange yellow fine powder
10.21
10.20
1
Orange yellow fine powder
10.21
10.19
2
Orange yellow fine powder
10.19
10.17
[0036] 3
Orange...
Embodiment 2
[0040] Mix 100 grams of lutein powder, 1170 grams of modified starch, 130 grams of sodium alginate, and 600 grams of Tween 60, add water three times the total weight of the above mixture, stir at 80°C for 1 hour, and control the speed at 300 rpm / minute, after cooling, filter the solution, and spray the filtrate to dry under the conditions of spray dryer pressure 1Mpa, inlet temperature 200°C, and outlet temperature 100°C to obtain cold water-dispersed lutein microcapsule powder with an average particle size of 100 μm .
[0041] The following are the experimental results of preparing lutein microcapsules with sodium alginate / modified starch / Tween 60
[0042] Lutein (g)
Embodiment 3
[0044]Mix 400 grams of lutein powder, 400 grams of modified starch, 600 grams of gum arabic, and 600 grams of Span 80, add water 15 times the total weight of the above mixture, stir at 30°C for 8 hours, and control the speed at 600 rpm , after cooling, the solution is filtered, and the filtrate is sprayed and dried under the conditions of a spray dryer pressure of 10 MPa, an inlet temperature of 120° C., and an outlet temperature of 50° C. to obtain an average particle size of 60 μm cold water-dispersible lutein microcapsule powder.
[0045] The following are the experimental results of preparing lutein capsules from gum arabic / modified starch / Span 80
[0046] Lutein (g)
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