Poly(ether-ether-ketone) composite material, production method and application of sealing member
A polyether ether ketone and composite material technology, which is applied in the parts, mechanical equipment, engine components, etc. in contact between the valve element and the valve seat, can solve the problems of poor hydrolysis resistance, easy breakage, leakage, etc. , good hydrolysis resistance, cost reduction effect
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Embodiment 1
[0026] Example 1: Making 30 seals with a size of 195 / Φ145×17 and a total of 10 kg.
[0027] 1. Raw material formula:
[0028] Polyetheretherketone powder 7.5kg
[0029] Nano particles 1kg
[0030] Polyperfluoroethylene propylene or polyphenylene sulfide 0.5kg
[0031] Glass fiber 1kg (fiber diameter is 6~12um, the ratio of length to diameter is 3:1~11:1)
[0032] 2. Mixing: It is mixed with a high-speed mixer, the mixing speed is 2000 rpm, and the mixing time is 2 minutes.
[0033] 3. Compression molding under the above conditions, sintering by gas heat-carrying sintering method, the highest sintering temperature is 380±10℃, the temperature is kept for 3 hours, and the temperature rise and fall speed is 50~80℃ / H.
[0034] 4. Secondary annealing treatment to eliminate material stress and deformation, temperature 200℃±20℃, time 2 hours.
[0035] 5. After checking the size, perform machining.
Embodiment 2
[0036] Example 2: Using carbon fiber to add up to 2kg can completely make a product, and meet and exceed the performance of the above example.
Embodiment 3
[0037] Embodiment 3: It is better to use a metal frame material for the seal, which can save the composite material of the present invention. cut costs.
[0038] Method embodiment, (1) Compression molding:
[0039] 1. Ingredients: 65 to 90 parts of polyether ether ketone, 10 to 30 parts of glass fiber, 2 to 10 parts of polytetrafluoroethylene, 5 to 10 parts of molybdenum disulfide, and 10 to 30 parts of carbon fiber. The above ratio is weight ratio.
[0040] 2. Mixing. According to the design requirements, pour the prepared materials into the automatic mixer for mixing and mixing. The mixing time is 0.5 to 1 minute, and the speed of the mixer is 2000 rpm.
[0041] 3. Press, add the mixed raw powder into the mold cavity, press at a speed of 20MPa / min at a room temperature of 20±5℃, the gauge pressure reaches 50MPa / cm 2 , Begin to deflate gradually, and then keep the pressure for 6 minutes to form the preform.
[0042] 4. Put the pressed preform into a special sintering furnace, and sin...
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