Methyl glycol fatty acid ester and preparation method thereof

A technology of propylene glycol fatty acid ester and propylene glycol, which is applied in the field of propylene glycol fatty acid ester and its preparation, can solve the problems of affecting consumers' purchasing desire, difficult to unify the quality of dairy products, volatile loss of fragrance, etc., and achieves excellent fragrance enhancement effect, wide Prospects for industrialization and the effect of stabilizing the product system

Inactive Publication Date: 2010-09-01
中原粮食集团多福多食品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the promotion of dairy products in China is not all smooth sailing. The reason is that the type and price are important. Lipid substances composed of different fatty acids, but their content in natural milk is often very low, which cannot reach the sensory threshold of people, resulting in insufficient frankincense and bad taste, which makes many people unwilling to drink milk
At present, the flavoring of dairy products mainly relies on adding flavors and spices to make up for the lack of flavor of dairy products or to cover up some peculiar smells. However, common flavors often need a certain period of time to penetrate into the dairy products, and the flavors are volatile. Fragrance is easy to volatilize and lose during storage, causing the product to have a different fragrance every day during the shelf life, so it is difficult to unify the quality of flavored dairy products
What's more important is that the products with added flavors can clearly feel the presence of flavors when tasting, especially when the flavors have not fully penetrated into the product, it will bring unreal feeling to consumers, until it affects palatability and affects consumers' purchase desire, which in turn affects sales
In addition, adding edible oil can also improve milk flavor, but the effect is limited

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0011] Example 1, Preparation of propylene glycol fatty acid ester: The weight parts of each raw material are: 0.1 parts of acetic acid, 0.02 parts of valeric acid, 3.0 parts of caproic acid, 40 parts of palmitic acid, 1 part of oleic acid, 1 part of linoleic acid, hard 50 parts of fatty acid, 55 parts of propylene glycol, 0.3 part of sodium carbonate.

[0012] The synthesis method is: in the presence of the catalyst sodium carbonate, first esterify propylene glycol, palmitic acid, oleic acid, linoleic acid, and stearic acid at 225℃ for 60 minutes, then lower the temperature to 210℃, and add valeric acid , Caproic acid is kept for 60 minutes for esterification, then the temperature is lowered to 190°C, acetic acid is added and kept for 120 minutes for esterification, and then the temperature is lowered to 120°C and the material is discharged to obtain the product of the present invention propylene glycol fatty acid ester.

Embodiment 2

[0013] Example 2, Preparation of propylene glycol fatty acid ester: wherein the parts by weight of each raw material are: 2.5 parts of butyric acid, 2.5 parts of valeric acid, 1 part of palmitic acid, 5 parts of linoleic acid, 10 parts of stearic acid, 1 part of oleic acid , 35 parts of propylene glycol, 1.0 part of potassium carbonate, 1.0 part of sodium bicarbonate, 1.0 part of potassium bicarbonate.

[0014] The synthesis method is: in the presence of the catalyst potassium carbonate, sodium bicarbonate, and potassium bicarbonate, first esterify propylene glycol, palmitic acid, linoleic acid, stearic acid, and oleic acid at 245℃ for 40 minutes, and then heat the temperature The temperature is lowered to 230°C, valeric acid is added, and the temperature is kept for 30 minutes for esterification, and then the temperature is lowered to 210°C, butyric acid is added for 60 minutes for esterification, and then the temperature is lowered to 120°C for discharging to obtain the product ...

Embodiment 3

[0015] Example 3 Preparation of propylene glycol fatty acid ester: wherein the weight parts of each raw material are: 1.3 parts of acetic acid, 1.5 parts of caproic acid, 3 parts of linoleic acid, 50 parts of stearic acid, 3 parts of palmitic acid, 80 parts of propylene glycol, hydrogen 1.7 parts of potassium oxide.

[0016] The synthesis method is: in the presence of the catalyst potassium hydroxide, first esterify propylene glycol, linoleic acid, stearic acid, and palmitic acid at 236°C for 55 minutes, then lower the temperature to 220°C, and add caproic acid for 60 minutes. It is esterified within minutes, then the temperature is lowered to 200°C, acetic acid is added and the temperature is kept for 60 minutes for esterification, and then the temperature is lowered to 120°C for discharging to obtain the propylene glycol fatty acid ester of the present invention.

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PUM

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Abstract

The invention discloses a propanediol fatty acid ester and the preparation method, which is characterized in that: the propanediol and A, B and C fatty acids are esterified under the alkaline catalysis to get the propanediol fatty acid ester; wherein, raw material A is one or two among acetic acid and ethyl acetic acid; raw material B is one or two among pentanoic acid and caproic acid; raw material C is at least three among palmitic acid, oleic acid, linoleic acid and stearic acid. The fatty acid and the propanediol according to different proportion composition are esterified according to certain technique and have excellent aroma-enhancing effect. The propanediol fatty acid ester and the preparation method has the advantages of not only improving quality of dairy products, enhancing taste, increasing the level of dairy products, but also stabilizing product system and having the role of avoiding milk fat precipitation and protecting protein.

Description

Technical field [0001] The invention belongs to the field of food additives, relates to a food emulsifier that can increase the milk flavor of dairy products, and particularly relates to a propylene glycol fatty acid ester and a preparation method thereof. Background technique [0002] Food emulsifiers are the most important type of food additives. In addition to their typical surfactant effects, they can also interact with carbohydrates, proteins and lipids in foods. They can be widely used in dairy products and meat. Various foods such as products, noodles, etc. The production and sales of dairy products in my country have grown rapidly, especially in recent years, with an average increase of more than 20%. Therefore, the dairy industry is a sunrise industry, and its development prospects are very optimistic. However, the promotion of dairy products in the country has not been smooth sailing. The reason is that the type and price are important. The taste of dairy products is ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07C67/08C07C69/003A23L1/035A23L29/10
Inventor 郑心羽乔占超
Owner 中原粮食集团多福多食品有限公司
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