Methyl glycol fatty acid ester and preparation method thereof
A technology of propylene glycol fatty acid ester and propylene glycol, which is applied in the field of propylene glycol fatty acid ester and its preparation, can solve the problems of affecting consumers' purchasing desire, difficult to unify the quality of dairy products, volatile loss of fragrance, etc., and achieves excellent fragrance enhancement effect, wide Prospects for industrialization and the effect of stabilizing the product system
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Embodiment 1
[0011] Example 1, Preparation of propylene glycol fatty acid ester: The weight parts of each raw material are: 0.1 parts of acetic acid, 0.02 parts of valeric acid, 3.0 parts of caproic acid, 40 parts of palmitic acid, 1 part of oleic acid, 1 part of linoleic acid, hard 50 parts of fatty acid, 55 parts of propylene glycol, 0.3 part of sodium carbonate.
[0012] The synthesis method is: in the presence of the catalyst sodium carbonate, first esterify propylene glycol, palmitic acid, oleic acid, linoleic acid, and stearic acid at 225℃ for 60 minutes, then lower the temperature to 210℃, and add valeric acid , Caproic acid is kept for 60 minutes for esterification, then the temperature is lowered to 190°C, acetic acid is added and kept for 120 minutes for esterification, and then the temperature is lowered to 120°C and the material is discharged to obtain the product of the present invention propylene glycol fatty acid ester.
Embodiment 2
[0013] Example 2, Preparation of propylene glycol fatty acid ester: wherein the parts by weight of each raw material are: 2.5 parts of butyric acid, 2.5 parts of valeric acid, 1 part of palmitic acid, 5 parts of linoleic acid, 10 parts of stearic acid, 1 part of oleic acid , 35 parts of propylene glycol, 1.0 part of potassium carbonate, 1.0 part of sodium bicarbonate, 1.0 part of potassium bicarbonate.
[0014] The synthesis method is: in the presence of the catalyst potassium carbonate, sodium bicarbonate, and potassium bicarbonate, first esterify propylene glycol, palmitic acid, linoleic acid, stearic acid, and oleic acid at 245℃ for 40 minutes, and then heat the temperature The temperature is lowered to 230°C, valeric acid is added, and the temperature is kept for 30 minutes for esterification, and then the temperature is lowered to 210°C, butyric acid is added for 60 minutes for esterification, and then the temperature is lowered to 120°C for discharging to obtain the product ...
Embodiment 3
[0015] Example 3 Preparation of propylene glycol fatty acid ester: wherein the weight parts of each raw material are: 1.3 parts of acetic acid, 1.5 parts of caproic acid, 3 parts of linoleic acid, 50 parts of stearic acid, 3 parts of palmitic acid, 80 parts of propylene glycol, hydrogen 1.7 parts of potassium oxide.
[0016] The synthesis method is: in the presence of the catalyst potassium hydroxide, first esterify propylene glycol, linoleic acid, stearic acid, and palmitic acid at 236°C for 55 minutes, then lower the temperature to 220°C, and add caproic acid for 60 minutes. It is esterified within minutes, then the temperature is lowered to 200°C, acetic acid is added and the temperature is kept for 60 minutes for esterification, and then the temperature is lowered to 120°C for discharging to obtain the propylene glycol fatty acid ester of the present invention.
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