High-efficiency energy-saving nano antiwear agent and preparation method and application thereof

A nano-anti-wear, high-efficiency and energy-saving technology, used in additives, base materials, petroleum industry, etc., can solve the problems of nano metal particle additives difficult to maintain chemical and physical stability for a long time, lubricating oil difficult to maintain dispersion stability for a long time, application restrictions and other problems , to achieve the effect of good cold start function, good dispersibility and not easy precipitation

Active Publication Date: 2009-03-11
石家庄劲力宝石油化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

It is worth noting that during the storage and use of lubricating oil, it is difficult for nano-metal particle additives with high chemical activity and surface activity to maintain chemical and physical stability for a long time,

Method used

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  • High-efficiency energy-saving nano antiwear agent and preparation method and application thereof

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Experimental program
Comparison scheme
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Embodiment 1

[0027]Embodiment 1: the nanometer antiwear agent of the present invention is to be made by the raw material of following weight ratio: 250 grams of nanometer metal microparticles, 5000 grams of cleaning and dispersing agents, 5000 grams of antioxidants, 3000 grams of organic high polymers, diluted Dosage 200,000 grams. Wherein, the above-mentioned nano-metal particles are metal particles molybdenum, boron, chromium, vanadium, titanium, aluminum, cerium, a mixture of two or more (that is, a combination of two or more), the particle size of the nano-metal particles 1 to 100nm. For example, the nano metal particles can be a combination of metal particles chromium and vanadium, or a combination of metal particles titanium, aluminum and cerium. The particle size of the nano metal particles may be 40-60 nm. Detergent and dispersant are calcium petroleum sulfonate with medium alkali value, barium polyisobutylene sulfur phosphate, calcium sulfide alkyl phenate, monosuccinimide ashle...

Embodiment 2

[0029] Embodiment 2: the nanometer antiwear agent of the present invention is to be made by the raw material of following weight ratio: 50 grams of nanometer metal microparticles, 100 grams of cleaning and dispersing agents, 100 grams of antioxidants, 300 grams of organic polymers, diluted Dosage 90000 grams. Wherein, the above-mentioned nano-metal particles are metal particles molybdenum, boron, chromium, vanadium, titanium, aluminum, cerium, a mixture of two or more (that is, a combination of two or more), the particle size of the nano-metal particles 1 to 100nm. For example, the nano-metal particles can be a combination of metal particles molybdenum and boron, or a combination of metal particles boron, chromium, vanadium, titanium, and aluminum. The particle size of the nano metal particles may be 70-80 nm, or may be 10-30 nm. Detergent and dispersant are calcium petroleum sulfonate with medium alkali value, barium polyisobutylene sulfur phosphate, calcium sulfide alkyl p...

Embodiment 3

[0030] Embodiment 3: the nanometer antiwear agent of the present invention is to be made by the raw material of following weight proportion: 500 grams of nanometer metal microparticles, 10000 grams of cleaning and dispersing agents, 9000 grams of antioxidants, 3500 grams of organic high polymers, diluted Dose 400,000 grams. Its preparation method is with embodiment 1 (or with embodiment 2).

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Abstract

The invention discloses a high-efficiency energy-saving nano anti-wear agent, a preparation method and application thereof. The nano anti-wear agent is made by the following raw materials in weight proportion: 1 to 500 portions of nano metal particles, 100 to 10,000 portions of detergent dispersant, 100 to 10,000 portions of antioxidant, 100 to 5,000 portions of organic high polymer, and 80,000 to 500,000 portions of diluting agent, wherein the nano metal particles are mixture of two or more than two of metal particle molybdenum, boron, chromium, vanadium, titanium, aluminum and cerium. The compositions are mixed according to the proportion, are stirred to react at a specified temperature, are circularly sprayed and dispersed for a plurality of hours through a high-pressure plunger pump, and then form a steady nano-metal eutectic ion organic compound colloid by the dispersion of a high-power ultrasonic device. The nano anti-wear agent has the advantages of good service performance, simple preparation method, and broad application, and can form novel lubricating oil series products with lubricating oil.

Description

technical field [0001] The invention relates to a nanometer antiwear agent, and also relates to a preparation method and application of the nanometer antiwear agent. Background technique [0002] Nanomaterials have attracted extensive attention due to their special physical and chemical properties, and have been initially applied in many fields. In the field of tribology, a great deal of research has been done on nanoparticulate lubricant additives. It has been found that a variety of nano-metal particles as additives can effectively improve the anti-friction, anti-wear and extreme pressure properties of oil. It is worth noting that during the storage and use of lubricating oil, it is difficult for nano-metal particle additives with high chemical activity and surface activity to maintain chemical and physical stability for a long time, and the easy agglomeration of nano-metal particles makes it difficult for them to be used in lubricating oil for a long time. Maintain disp...

Claims

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Application Information

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IPC IPC(8): C10M101/00C10M141/08C10M143/00C10N30/06
Inventor 王长青
Owner 石家庄劲力宝石油化工有限公司
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