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Method for preparing high-hardness pulp by using grass type plants as raw materials

A technology of plant raw materials and grasses, applied in the field of high hardness pulp and its preparation, can solve the problems of papermaking hazards, difficult recycling, and large energy consumption

Active Publication Date: 2009-06-10
SHANDONG FUYIN PAPER & ENVIRONMENTAL PROTECTION TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

3. Due to the high content of silicon and carbohydrates in the raw materials, the viscosity of the black liquor is high and the recovery is difficult
4. Grasses now contain a large number of miscellaneous cells, which pose a series of hazards to papermaking
[0012] The second issue of Chemical Industry Times in 2002 published an article entitled "Research on Straw Low-pressure and Low-temperature Pulping". The article used rice straw as raw material to obtain bleached pulp through the steps of pre-impregnation, cooking, washing and sieving, and bleaching. Keep warm for up to 3.5 hours, requiring a lot of energy

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0075] The straw after the dry preparation is passed through the dipping screw machine, and the dipping liquid is added in the dipping screw machine, wherein the amount of alkali used is 16% based on sodium hydroxide and the amount of absolute dry straw, and then sent into steaming balls, anthraquinone The addition amount is 0.6% of the absolute dry raw material, the liquid ratio is 1:3, and the steaming ball is idling for 20 minutes after the straw is filled; after that, the steam is heated once to raise the temperature to 100°C, and the temperature is kept at this temperature for 25 minutes, and then Let off steam for 20-30 minutes, start steaming after secondary heating, raise the temperature for 30 minutes to 165°C, and keep warm for 55 minutes; before spraying, add black liquor to the steaming ball to dilute, while maintaining the pressure at 0.75MPa for spraying Put, the hardness of pulp at this moment is potassium permanganate value 20 is equivalent to Kappa value 32, an...

Embodiment 2

[0077] Carry out the wheat straw after the dry preparation of materials through the hammer crusher into the steaming ball, add the cooking liquid in the steaming ball, wherein the amount of alkali used is 18% of the absolute dry raw material amount in terms of sodium hydroxide, and the addition of anthraquinone is The absolute dry raw material is 0.7%, the liquid ratio is 1:4, the steaming ball is idling for 20 minutes after the wheat straw is filled; after that, the steam is heated once to raise the temperature to 110°C, and the temperature is kept at this temperature for 20 minutes, and then the steam is released. After 20-30 minutes, the second heating starts to pass steam, and the temperature is raised for 30 minutes to 168°C, and the temperature is kept for 40 minutes; before spraying, add black liquor to the steaming ball for dilution, and at the same time keep the pressure at 0.75MPa for spraying. The hardness of pulp is 18 for potassium permanganate value, which is equi...

Embodiment 3

[0079] After the dry preparation, the straw is passed through the dipping screw machine, and the dipping liquid is added to the dipping screw machine, wherein the amount of alkali used is 20% of the absolute dry straw amount based on sodium hydroxide, mixed and dipped, and then sent to steaming balls, anthracene The amount of quinone added is 0.8% of the absolute dry raw material, the liquid ratio is 1:2.5, and the steaming ball is idling for 20 minutes after the straw is filled; after that, the steam is heated once to raise the temperature to 120°C, and the temperature is kept at this temperature for 25 minutes. Let off steam for another 20-30 minutes, start steaming for the second heating, raise the temperature for 30 minutes to 173°C, and keep warm for 35 minutes; before spraying, add black liquor to the steaming ball to dilute, while maintaining the pressure at 0.75MPa Spraying, the hardness of this moment pulp is that potassium permanganate value 16 is equivalent to Kappa ...

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PUM

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Abstract

The invention discloses a method for preparing high-hardness pulp by taking a grass plant as a raw material. The method comprises the steps of material preparation and stewing, the prepared raw material is conveyed into a digester to be stewed into the high-hardness pulp of which the hardness has a potassium permanganate value of between 16 and 28 and is equivalent to a Kappa number of between 24 and 50, a stewing method comprises that the grass plant raw material is prepared and then enters an impregnation screw to be conveyed into the digester, and a stewing reagent is added into the digester; steam is aerated to heat, and the thermal insulation is performed for the needed time when the needed pressure is achieved by heating. Compared with the prior art, the stewing and thermal insulation time of the method is greatly shortened, which greatly reduces energy consumption for enterprises and improves production efficiency; and the prepared high-hardness pulp can be taken as a raw material for preparing bleached chemical pulp.

Description

[0001] This application is a divisional case of an application with the application number 200710300209.X, the application date is December 5, 2007, and the invention name is "a pulp and black liquor prepared from grass raw materials, its preparation method and its application" Apply. technical field [0002] The invention relates to a high-hardness pulp, more specifically, to a high-hardness pulp prepared from grass plants and a preparation method thereof. Background technique [0003] The methods of producing pulp from plant fibers are: chemical method, mechanical method and chemical mechanical method. Chemical pulping is the use of chemical action to dissociate raw materials into pulp by removing certain components in plant fiber raw materials. It is the most widely used pulping method. In chemical cooking, it is divided into lime method, caustic soda method, and anthracene method. Quinone-caustic soda method, sulfate method, sulfite method cooking. [0004] The sulfite...

Claims

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Application Information

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IPC IPC(8): D21C3/00D21C3/14D21C3/02D21H11/12D21C7/00D21H17/05D21H17/66D21B1/06
Inventor 李洪法杨吉慧宋明信陈松涛宋建军
Owner SHANDONG FUYIN PAPER & ENVIRONMENTAL PROTECTION TECH
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