Reception device and reception method
A recording medium, inkjet recording ink technology, applied in the direction of copying/marking method, ink, printing, etc., can solve the problem of poor inkjet stability, difficult ink with high viscosity reliability and ease of operation, maintenance of inkjet equipment Problems such as equipment damage
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preparation Embodiment 1
[0361] -Preparation of water-soluble polymer compound aqueous solution A-
[0362] α-olefin-maleic anhydride copolymer represented by the following structural formula (II) (T-YP112, manufactured by SEIKO PMC Corporation, its olefin chain (R): 20 to 24 carbon atoms, acid value 190 mgKOH / g and weight The average molecular weight is 10,000): 10.0 parts by mass
[0363] Structural formula (II)
[0364] In the structural formula (II), R represents an alkyl group. "n" represents an integer of 30 to 100.
[0365] ●Standard LiOH aqueous solution (the amount of acid value is 1.2 times of the α-olefin-maleic anhydride copolymer represented by structural formula (II): 17.34 parts by mass
[0366] ●Ion-exchanged water: 72.66 parts by mass
[0367] [278] Subsequently, the mixture is heated and stirred with a stirrer to dissolve the α-olefin-maleic anhydride copolymer shown in the structural formula (II), and filter out a very small amount of undissolved matter through a filter with a...
preparation Embodiment 2
[0369] -Preparation of Surface-treated Black Pigment Dispersion Solution-
[0370] [279] Add 90g carbon black in 3,000ml 2.5N sodium sulfate solution, the carbon black has 150m 2 The specific surface area of CTAB / g and the oil absorption of DBP 100mL / 100g; then, at a temperature of 60°C, the mixture was stirred at a rotation speed of 300rpm and allowed to react for 10 hours, whereby the carbon black was oxidized. The reaction solution was filtered, and the filtered carbon black was then neutralized with sodium hydroxide solution and subjected to ultrafiltration.
[0371] [280] The obtained carbon black was washed with water, dried, and dispersed in purified water so that the solid content was 30% by mass, and the mixture was sufficiently stirred to obtain a black pigment dispersion solution. Measure the average particle diameter (D) of the pigment dispersed phase in this black pigment dispersion solution 50 ) is 103nm. In addition, the average particle diameter (D 50 ). ...
preparation Embodiment 3
[0373] -Preparation of polymer fine particle dispersion solution containing magenta pigment-
[0374]
[0375] [281] The gas in a 1L flask equipped with a mechanical stirrer, a thermometer, a nitrogen introduction tube, a reflux tube and a dropping funnel was fully replaced with nitrogen, and then 11.2g styrene, 2.8g acrylic acid, 12.0g lauryl methacrylate, 4.0 g of polyethylene glycol methacrylate, 4.0 g of styrene macromonomer and 0.4 g of mercaptoethanol were mixed together and heated to 65°C.
[0376][282] Subsequently, will include 100.8g styrene, 25.2g acrylic acid, 108.0g lauryl methacrylate, 36.0g polyethylene glycol methacrylate, 60.0g hydroxyethyl methacrylate, 36.0g styrene macromolecule A mixed solution of the monomer, 3.6 g of mercaptoethanol, 2.4 g of azobismethyl valeronitrile and 18 g of methyl ethyl ketone was added dropwise into the flask for 2.5 hr. Thereafter, a mixed solution including 0.8 g of azobismethylvaleronitrile and 18 g of methyl ethyl ketone w...
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