One-dimensional rod-like mesoporous material and preparation method thereof and application thereof
A mesoporous material and rod-shaped technology, applied in the field of mesoporous materials, can solve the problems of high raw material cost, poor hydrothermal stability, long one-dimensional rod-shaped mesoporous material, etc., and achieve the effect of simple process steps and low cost
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Embodiment 1
[0035] Preparation of MCM-41 One-dimensional Rod Mesoporous Material
[0036] Mix 7.68g of absolute ethanol, 11.57g of tetraethyl orthosilicate and 1ml of hydrochloric acid (2.8mmol / L), stir slowly and evenly, condense and reflux for 90min in a water bath at 60°C; then add 15g of absolute ethanol, 1.52g Cetyltrimethylammonium bromide (CTAB), 4ml of hydrochloric acid (55mmol / L) mixed solution, stirred at room temperature 25 ° C for 30 minutes, cooled to room temperature 25 ° C to obtain a precursor solution containing CTAB . Using a suction filter pump (produced by Shanghai Mosu Scientific Equipment Co., Ltd., HPD-25 type oil-free suction filter pump) and a standing suction filter device (1000ml suction filter bottle) in the laboratory, the precursor solution of 6ml (containing CTAB) was divided into three times ( 2ml each time) was filtered through a porous polycarbonate membrane (produced by Whatman Company, UK, with a membrane diameter of 47mm, a pore diameter of 200μm, and...
Embodiment 2
[0044] Preparation of SBA-15 One-Dimensional Rod Mesoporous Materials
[0045] 15g of absolute ethanol, 0.10g of hydrochloric acid (12mol / L) and 2.0g of deionized water were mixed uniformly and placed in a three-necked flask, then, under slow stirring, 1.0g of surfactant P123 was added to the mixed solution until P123 was completely dissolved, and the three-necked flask containing the mixed solution was placed in an oil bath, and at a temperature of 60°C, after slowly stirring for 1 h, 2.13 g of tetraethyl orthosilicate was gradually added dropwise, and at 60 ℃ oil bath temperature for 12h with stirring and aging, and then cooled to room temperature to obtain the precursor solution containing P123. Using a suction filter pump (produced by Shanghai Mosu Scientific Equipment Co., Ltd., HPD-25 type oil-free suction filter pump) and a standing suction filter device (1000ml suction filter bottle) in the laboratory, the precursor solution of 6ml (containing P123) was divided into th...
Embodiment 3
[0053] Put the SBA-15 type one-dimensional rod-shaped mesoporous silica material generated by six organic-inorganic composite mesoporous membranes into 5ml, 0.04mg / ml aqueous solution of horseradish peroxidase, and pass the ultraviolet-visible spectrophotometry Detect the absorbance change of the horseradish peroxidase solution soaked with the mesoporous material at 402nm (the visible maximum absorption peak of the horseradish peroxidase), and the change of the absorbance is related to that of the horseradish peroxidase in the mesoporous The adsorption of the material is directly related.
[0054] by attaching Figure 7 It can be observed that the absorbance of the horseradish peroxidase solution at 402nm (the visible maximum absorption peak of the horseradish peroxidase) is along with the SBA-15 type one-dimensional rod-shaped mesoporous silica material in the horseradish peroxidase The increase of soaking time in the solution gradually decreased, and basically reached stabi...
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