Recovery and comprehensive utilization method of heavy metals in stainless steel pickling wastewater sludge
A technology of pickling wastewater sludge and recovery method, which is applied in water/sludge/sewage treatment, sludge treatment, chromium oxide/hydrate, etc., and can solve the difficulty of increasing the comprehensive utilization of wastewater heavy metal sludge and the fluctuation of metal content Large-scale, secondary pollution of the ecological environment and other problems, to achieve the effects of environmental protection and resource conservation, comprehensive utilization, resource utilization and comprehensive utilization, and cost savings
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[0029] The present invention adopts a wet process to treat sludge from stainless steel pickling wastewater treatment. The process flow mainly includes acid leaching, neutralization and precipitation, extraction, and reuse of recovered heavy metals in stainless steel smelting, and proceed as follows:
[0030] (1) Put the heavy metal sludge in the first reactor, add the waste pickling solution, stir, and control the end-point pH within the range of 1.0 to 1.5, fully leaching the reaction, filtering, and pumping the filtrate into the second reaction In the tank, the filter residue is treated separately.
[0031] (2) Add sodium fluoride solution to the second reaction tank, adjust the pH of the solution within the range of 4.0-4.5, fully react, filter, pump the filtrate into the third reaction tank, and treat the residue separately. This step will remove calcium, magnesium, and aluminum impurities in the filtrate.
[0032] (3) Add sodium hydroxide alkali solution to the third reaction t...
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