Barium chloride production technology
A production process, barium chloride technology, applied in the direction of calcium/strontium/barium chloride, calcium/strontium/barium halide, etc., can solve the problem that impurities are difficult to completely remove, do not meet the needs of large-scale industries, and impurities are easy to enter, etc. problems, to achieve the effect of reducing pollution and waste of resources, adapting to large-scale industrial production, and low impurity content in products
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[0029] Example 1: According to the weight percentage of the barium carbonate contained in the asperite containing 65% by weight, the asperite: hydrochloric acid: water: hydrogen peroxide is fed into the reactor 2 at a uniform rate and the mixture 1 of hydrochloric acid: water: The weight percentage concentration is 30-32%, and the weight percentage concentration of hydrogen peroxide is ≥29%. Free sulfur (S) and iron (Fe) react with hydrogen peroxide to form a precipitate. After the reaction no carbon dioxide is released, centrifuge for 4 The filter residue, the filtrate is a hydrated barium chloride raw material liquid, the released carbon dioxide is recovered and purified through outlet 3 to produce barium carbonate, and the filter residue is used as a cement additive; the raw material liquid is fed into the crystallization kettle 21 through the raw material pump 5, and the electric heating temperature control device 13 heats and controls Keep the temperature in the crystalliza...
Example Embodiment
[0039] Example 3: Repeat Example 1 according to the same steps described above, but with 50% barium carbonate contained in asperite, mixing asperite: hydrochloric acid: water: hydrogen peroxide in a ratio of 1.3:0.37:1:0.1 and inputting it into the reaction at a constant rate In kettle 2, a chemical reaction occurs. The obtained product barium chloride is the same as in Example 1.
Example Embodiment
[0040] Example 4: Repeat Example 1 according to the same steps as described above, but the asperite contains barium carbonate based on 70% by weight, and the asperite: hydrochloric acid: water: hydrogen peroxide is mixed at a ratio of 0.93:0.37:1:0.1 and fed into the reaction at a constant speed In kettle 2, a chemical reaction occurs. The obtained product barium chloride is the same as in Example 1.
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