Method for manufacturing high-purity metal wire

A manufacturing method and metal wire technology are applied in the field of directly using electrolytic metal plates to prepare high-purity metal wires, which can solve the problems of long production cycle, high cost and difficulty of copper wires, shorten the production cycle, eliminate pollution problems, and avoid The effect of material loss

Inactive Publication Date: 2010-08-11
江西江镍高纯材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] 1. In the process of smelting and casting ingots, iron, manganese, titanium, silicon, carbon, rare earth and other auxiliary materials need to be added, which increases the impurity content in the finished nickel wire. Generally, the impurity content in the nickel wire reaches about 0.5%. In addition to reducing the purity of the material, it is also very easy to form inclusions in the nickel wire, which increases the resistivity of the nickel wire and deteriorates the plasticity, making it difficult to meet the processing and application requirements of metal wires for electronic products;
[0006] 2. There are many production links, large investment in equipment, and a large production area;
[0007]3. Long production cycle
Generally, it takes 7 days from feeding materials to finished products, and the production efficiency is low;
[0008] 4. High energy consumption
[0009] 5. During the smelting process, since the smelting temperature is above 1500°C, and the temperature of the subsequent two thermal processing is around 1000°C, there will be more than 2% loss in the production process
[0010] 6. The product qualification rate is low
[0011] The production process of conventional pure copper wire is similar to the preparation process of the above-mentioned pure nickel wire, and there is also the phenomenon that the material purity is reduced due to easy doping during the smelting process, so the cost and difficulty of preparing ultra-high-purity copper wire are high.

Method used

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  • Method for manufacturing high-purity metal wire

Examples

Experimental program
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Embodiment 1

[0040] Embodiment 1, as figure 2 As shown, this embodiment takes the preparation of high-purity nickel wire as an example to describe the present invention in detail. This embodiment includes the following steps:

[0041] S1. Firstly, the electrolytic nickel raw material plate is cut and pre-degassed to form a raw nickel strip, wherein the degassing treatment is dehydrogenation and desulfurization treatment.

[0042] In this embodiment, the high-purity electrolytic nickel raw material plate is cut into nickel strips first, and then subjected to dehydrogenation and desulfurization treatment; the electrolytic nickel raw material plate can also be subjected to dehydrogenation and desulfurization treatment first, and then divided into nickel strips.

[0043] Dehydrogenation and desulfurization treatment is: place the slit nickel strip or unslit electrolytic nickel raw material plate in a gas or diesel combustion box-type heating furnace, heat it to 300°C, and heat it at this tem...

Embodiment 2

[0067] Embodiment 2, as image 3 As shown, a high-purity nickel wire was prepared. Steps S1-S5 of this embodiment are the same as those of Embodiment 1, and steps S1-S5 will not be described in detail here.

[0068] When the user needs non-soft high-purity metal wire for delivery, before the high-purity metal wire is drawn to the wire diameter of the finished high-purity metal wire, continuous annealing treatment before the finished product is carried out, and then the wire is drawn to the wire diameter of the finished high-purity metal wire size. Specifically, the continuous annealing treatment before the finished product is an annealing treatment by directly passing an electric current on the high-purity metal wire. , the larger the current is. After continuous annealing treatment before the finished product, it is passed through the finished product mold, that is, it is drawn to the required product high-purity metal wire diameter size by a single-mode or multi-mode wire...

Embodiment 3

[0074] Example 3, such as image 3 As shown, a high-purity nickel wire was prepared. In this embodiment, the annealing treatment before the post-finished product in the step S5 adopts continuous annealing treatment in a tube furnace. All the other steps are with embodiment 1.

[0075] The pre-finished product annealing treatment in this embodiment selects continuous annealing treatment in a tube furnace under a reducing atmosphere of ammonia decomposition gas, wherein the annealing temperature is 650°C-850°C, and the annealing speed is 2m / min-6m / min. The larger the diameter of the high-purity metal wire, the slower the annealing speed and / or the higher the annealing temperature. The specific annealing parameters of the tube furnace are shown in Table 7.

[0076] Table 7

[0077] diameter (mm)

[0078] When the diameter is less than 1mm, an annealing speed of 5m / min at 650°C can also be selected.

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Abstract

The invention discloses a method for manufacturing a high-purity metal wire. The method comprises the following steps: S1, performing slitting and degassing pretreatment on an electrolyzed raw material plate to form a raw material metal strip; S2, rolling the raw material metal strip to manufacture a semi-finished product of the high-purity metal wire; S3, annealing the semi-finished product of the high-purity metal wire; S4, carrying out cold-press welding on a plurality of annealed semi-finished products of the high-purity metal wires to ensure that the metal wires are connected end to end in sequence; and S5, coldly drawing the semi-finished product of the high-purity metal wire which is subjected to cold press welding to directly form a finished product of the high-purity metal wire; or continuously annealing the metal wire before the high-purity metal wire is drawn to the size of wire diameter of the finished product of the high-purity metal wire, and drawing the metal wire to the size of the wire diameter of the finished product of the high-purity metal wire. The invention provides the high-purity metal wire manufacturing method with the advantages of high production efficiency, low energy consumption, little investment and simple process, and the manufactured high-purity metal wire has the characteristics of high purity, high conductivity, good manufacture performance and the like.

Description

technical field [0001] The invention relates to a method for manufacturing high-purity metal wires, in particular to a method for directly using electrolytic metal plates to prepare high-purity metal wires. Background technique [0002] High-purity metal wires (including high-purity copper wires, high-purity nickel wires, etc.) are widely used in the manufacturing industry of electronic and electrical products, such as high-definition TV signal lines, high-quality audio A large number of high-purity metal wires are used. Physical parameters such as diameter, purity and ductility of high-purity metal wires are key factors affecting the quality of electronic and electrical products based on them. With the development trend of miniaturization and high performance of electronic and electrical products, high-purity metal wires are required to have higher purity, better ductility, thermal conductivity and lower resistance value. [0003] Such as figure 1 Shown is a conventional...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B23P15/00
Inventor 林榆滨徐卓辉
Owner 江西江镍高纯材料有限公司
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