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Preparation process and device of nano-particle reinforced bimetal composite

A nanoparticle, composite technology

Inactive Publication Date: 2010-12-15
丁家伟
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, although many preparation methods of metal surface composite materials have been developed at home and abroad, each method has its shortcomings that are difficult to overcome.
For example, the coating and the substrate in the spraying technology are still mechanically combined, and the sprayed layer falls off, which is not suitable for heavy-duty operating conditions; in the high-energy beam heat source cladding, the problem of pores and opening of the cladding layer has always been a difficult problem for carbide ceramic surfacing Cracks on the surfacing welding surface, low hardness on the spray welding surface, uneven thickness of the spray welding layer, low utilization rate of spray powder, low coating bonding strength, and low coating density; there are more evaporation of alloying elements and decarburization in vacuum cladding The phenomenon and equipment are complex; the high-frequency induction fusion coating has the disadvantages of serious oxidation of the workpiece, rough surface, burning of alloy elements and weak bonding between the coating and the substrate, etc., which directly affect the production efficiency and service life of the product. It restricts its promotion and application; while the high-energy melting-injection technology is still in the stage of experimental exploration and has not yet reached the level of widespread application
[0010] It can be seen from the above-mentioned published patents and reports that although many surface nano-coating technologies have been developed at home and abroad, because the coated material layer is relatively thin, generally only 0.1-1mm thick, and the surface coating The bonding strength between the coated material and the base material is poor, and there are various disadvantages such as complex process and poor working environment, so that the coatings prepared by these processes are limited to a certain extent in terms of popularization and application.

Method used

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  • Preparation process and device of nano-particle reinforced bimetal composite
  • Preparation process and device of nano-particle reinforced bimetal composite
  • Preparation process and device of nano-particle reinforced bimetal composite

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] Example 1: figure 1 This equipment is a vacuum induction melting equipment. The equipment consists of box cover 1, workpiece 2, coating 3, protective coating 4, frequency conversion induction heater 5, manufacturing sand 6, vacuum pump valve 7, vacuum pump 8, vibrator 9, pipeline 10, box 11, frequency conversion induction heating The vibrator 5 is installed outside the box body 11, and the vibrator 9 is installed on the bottom or side of the box body 11. The vibrator 9 is mechanical vibration or ultrasonic vibration, and the frequency of the variable frequency induction heater 5 can be segmented from 500Hz to 200kHz. Stepless adjustment, the vacuum pump 8 is installed on any side of the box body 11, and is connected with the vacuum pump valve 7 and the vacuum pump 8 through the pipeline 10.

[0043] When the work starts, first set the mass percentage content as 20%Cr; 10%Ni, 2.5%Mo, 1.3%Si, 2.4%Mn, 1.8B%, 0.5%MgO, 0.4%CaF 2 , 0.3% C, 0.2% Nb, 0.5% CeO 2 , the balance...

Embodiment 2

[0044] Example 2: In figure 2 in, with figure 1 The difference is that the frequency conversion induction heater 5 is installed in the box body 11 .

[0045] At the beginning of the work, the mass percentage content is 15%Cr; 15%Ni, 3%Mo, 1.8%Si, 2.4%Mn, 2.0B%, 0.7%MgO, 0.5%CaF 2 , 0.47% C, 0.38% Nb, 0.4% Y 3 o 2 , 0.2% Co, and the balance is Fe. Put the raw materials of the above components into the mixer according to the ratio of the ingredients and mix them thoroughly. The mixing time is 4 hours to prepare an alloy powder, and then add it to the alloy powder of the above ingredients WC nanoparticles with a mass percentage content of 35% are prepared into a mixed alloy powder containing WC nanoparticle reinforcement, or prepared into a micro-nano hybrid alloy powder containing WC nanoparticle reinforcement through a stirring ball milling process in a stirring ball mill; Add 6% gasoline rubber solution adhesive to the above-mentioned alloy powder to prepare an alloy past...

Embodiment 3

[0047] Example 3: image 3 It is a vacuum induction cladding equipment. and figure 1 and figure 2 The difference is: the equipment consists of particle feeders 12 and 14, workpiece 13, alloy powder 15, molding die 16, molten pool 17, bimetallic composite and cladding layer 18, frequency conversion induction heater 19, bottom plate 20 , a lifting device 21, an inert gas delivery pipe 22 and a vibrator 26, wherein the number of particle feeders 12 and 14 is 1 to 8, installed on the upper part of the molding die 16, and the frequency conversion induction heater 19 is installed on the top of the molding die 16 Externally, the bottom plate 20 and the lifting device 21 are installed on the lower part of the molding die 16, the vibrator 26 is installed on the lower part or the upper part or the side of the molding die, the inert gas delivery pipe 22 is installed on the upper part of the molding die 16, and the molding die is divided into double open and close metal Water-cooled c...

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Abstract

The invention relates to a preparation process and a device of a nano-particle reinforced bimetal composite, the nano-particle reinforced bimetal composite comprises the following chemical components by weight percent: 6-25% of Cr, 4-18% of Ni, 1.0-4% of Mo, 1.0-1.8% of Si, 1.2-3% of Mn, 0.4-2.2% of B, 0.1-1.2% of MgO, 0.2-2% of CaF2, 0.2-0.7% of C, 0.2-0.8% of Nb, not more than 0.9% of one or the combination of CeO2, Y3O2 and La2O3, 0.0-0.8% of Co, and the balance of Fe, and mixed particles of nano-sized carbides, nitrides, borides or carbonitrides are added in alloy powder. The vacuum induction melting and the cladding processes and equipment are adopted for melting and cladding the mixture on a workpiece, the thickness of a cladding layer is 0.1-25mm, the cladding layer contains 1%-50% of nano-reinforcing particles of one or the combination of the carbides, the nitrides, the borides and silicides, and the cladding layer has special performances of wear resistance, corrosion resistance, electrical conductivity, self-lubrication performance and the like. A coating layer and a base material form the metallurgical bonding, thereby having high bonding strength, overcoming the drawbacks in various coating processes at home and abroad, leading the coating layer to avoid the defects of shrinkage cavities, inclusion, cracking, shedding and the like and having the advantages of high heating temperature, fast speed, high production efficiency, small energy consumption, simple preparation process and low cost.

Description

technical field [0001] The invention belongs to the technical field of metal-based composite materials, and relates to a nanoparticle-reinforced bimetallic composite material and a preparation method thereof, in particular to a nanoparticle-reinforced bimetallic composite material preparation process and equipment. Background technique [0002] Wear and corrosion are the main forms of failure of many parts and equipment, involving various fields of people's lives such as industry, agriculture, and military industry. The economic losses they cause are staggering. According to incomplete statistics, the direct losses caused by wear and corrosion every year About 1% to 4% of the gross national product. The losses caused by friction and wear of various mechanical parts all over the world are as high as hundreds of billions of dollars every year. Most of the wear and corrosion are from the surface of the material or from the surface, such as corrosion, wear, oxidation and fatigu...

Claims

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Application Information

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IPC IPC(8): C23C24/10
Inventor 丁家伟丁刚耿德英孙健强颖怀谢宗翰郭长庆
Owner 丁家伟
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