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Chip type oxygen sensor and preparation method thereof

An oxygen sensor and chip technology, applied in the field of chip oxygen sensor and its preparation, can solve the problems of short service life, low sensitivity of oxygen sensor, poor thermal shock resistance, etc., achieve long service life, improve sensitivity, and enhance adhesion Effect

Active Publication Date: 2013-07-03
BYD CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The invention solves the technical problems of low sensitivity, poor thermal shock resistance and short service life of the oxygen sensor existing in the prior art

Method used

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  • Chip type oxygen sensor and preparation method thereof
  • Chip type oxygen sensor and preparation method thereof
  • Chip type oxygen sensor and preparation method thereof

Examples

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preparation example Construction

[0025] The present invention also provides a preparation method of a chip oxygen sensor, comprising the following steps:

[0026] 1) Coating insulating layer slurry, electrode slurry, and insulating layer slurry on the heater substrate, drying, forming an insulating layer on the heater substrate, and obtaining the first sheet; getting a reference gas substrate as second sheet;

[0027] 2) screen-print the transition layer slurry on the oxygen measuring electrolyte layer to form a transition layer; the transition layer slurry contains zirconia, magnesium aluminum spinel and the first pore-forming agent; screen-print the porous layer slurry to form a transition layer; A porous layer is formed on the layer; the porous layer slurry contains zirconia, magnesium aluminum spinel, noble metal and the second pore-forming agent; the third layer is obtained; take a zirconia casting sheet and laser drill holes to obtain a dense Layer, as the fourth layer;

[0028] 3) One side of the ins...

Embodiment 1

[0042] (1) The heater substrate, the reference gas substrate blank, and the zirconia electrolyte matrix are prepared by casting technology; the insulating layer, the heating electrode, and the insulating layer are successively coated on the heater substrate by a screen printing process. The heater substrate is used as the first layer; the reference gas substrate blank is laser cut out of the air channel to make the reference gas substrate as the second layer; the oxygen measuring electrolyte is made by printing the upper electrodes on both sides of the zirconia electrolyte substrate Floor.

[0043] (2) Raw material preparation:

[0044] Transition layer slurry: (a) powder material: 65 parts by weight of zirconia; 27 parts by weight of magnesium aluminum spinel; 5 parts by weight of activated carbon (particle size: 1.8-4 μm) as a pore forming agent; 3 parts by weight of sintering aid ( Wherein aluminum oxide 1 weight part, magnesium oxide 1 weight part, calcium oxide 1 weight ...

Embodiment 2

[0050] The same method as in Example 1 is used to prepare the chip oxygen sensor of this example, the difference is that in step (4), the area of ​​the zirconia casting sheet is larger than that of the transition layer and the porous layer, and the porous layer is completely covered. Floor.

[0051] Through the above steps, the chip oxygen sensor of this embodiment is obtained, which has figure 1 The structure shown, in which the porous protective layer has Figure 4 The structure shown is denoted as A2.

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Abstract

The invention provides a chip type oxygen sensor and a preparation method thereof. A porous protection layer of the chip type oxygen sensor comprises a transition layer, a porous layer and a compact layer; holes are formed on all the layers, so that the bottom of the porous protection layer is communicated with the top of the porous protection layer; the transition layer contains zirconium oxide and magnesia alumina spinels, the average hole diameter of the transition layer ranges from 0.1 mu.m to 2.5 mu.m, and the porosity of the transition layer ranges from 20 percent to 40 percent; the porous layer contains zirconium oxide, magnesia alumina spinels and noble metal, the average hole diameter of the porous layer ranges from 0.1 mu.m to 3.5 mu.m, and the porosity of the porous layer ranges from 30 percent to 50 percent; and the compact layer contains zirconium oxide, the average hole diameter of the compact layer ranges from 2 mu.m to 3 mu.m, and the porosity of the compact layer ranges from 20 percent to 40 percent. Compared with the prior art, the chip type oxygen sensor has the advantages of high sensitivity and thermal shock resistance and long service life.

Description

technical field [0001] The invention relates to the field of automobile oxygen sensors, in particular to a chip oxygen sensor and a preparation method thereof. Background technique [0002] The oxygen sensor is used to detect the oxygen content in the exhaust gas exhausted by the engine. The flat-plate automotive zirconia oxygen sensor has the advantages of small size, fast response, low energy consumption, easy integrated heating and stable operation. During use, gasoline and engine oil contain lead, sulfur, phosphorus and other impurities, which will greatly reduce the performance of the sensor, while dust, oil, silicon and other components will block the protective layer and electrodes of the sensor, and lose the three-phase electrode reaction. The interface slows down the response speed of the oxygen sensor, and the signal output is insensitive, that is, the electrode is poisoned. In order to prevent electrode failure, the following two measures are generally adopted at...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N27/409B32B3/24
Inventor 徐斌王田军
Owner BYD CO LTD
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