Storable plant oil-based polyurethane wood adhesive and preparation method and application thereof
A wood adhesive and vegetable oil-based technology, which is applied in the field of vegetable oil-based polyurethane wood adhesives, can solve the problems of inconvenient application of adhesives, short storage time, and low environmental protection benefits, and achieve low cost and high synthetic process. Simple, large consumer market effect
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[0038] Example 1
[0039] Add 200g of commercially available vegetable oil polyol into a 500mL three-necked flask, stir and heat up to 50°C, evacuate to a vacuum of 0.08MPa, control the temperature to 105°C for dehydration for 3h, until no bubbles escape, cool to below 40°C, and put it in storage In the container with A4 molecular sieve, the moisture and impurities are further removed to obtain 187 g of dehydrated vegetable oil polyol, which is put into the dryer for later use. The vegetable oil polyols used in the following examples can all be dehydrated in this way.
Example Embodiment
[0040] Example 2
[0041] Add 200g of commercially available vegetable oil polyol into a 500mL three-necked flask, stir and heat to 60℃, evacuate to a vacuum of 0.1MPa, control the temperature to 125℃ for dehydration for 2h, until no bubbles escape, cool to below 40℃, and put it in storage In the container with A4 molecular sieve, the moisture and impurities are further removed to obtain 182 g of dehydrated vegetable oil polyol, which is put into the dryer for later use. The vegetable oil polyols used in the following examples can all be dehydrated in this way.
[0042] Method for preparing storable vegetable oil-based polyurethane wood adhesive
Example Embodiment
[0043] Example 3
[0044] 500g polymerized PAPI with a mass percentage of free isocyanate groups of 28%, 378.5g dehydrated soybean oil polyol prepared according to the method in Example 1, the dehydrated soybean oil polyol, each molecular chain contains 3.5 hydroxyl groups, weight average The molecular weight is 780, the hydroxyl value is 250mgKOH / g, the acid value is 0.08mgKOH / g, the viscosity (25°C) is 80mPa·s, the mass percentage of water content is 0.06%, and 188.3g of acetone is mixed in a three-necked bottle. 0.24g of dibutyltin dilaurate was dissolved in 1g of acetone and then added dropwise to a three-necked flask, filled with nitrogen protection, stirred for 25min, slowly heated to 80℃, reacted for 2h, the viscosity of the reaction solution reached 300mPa·s, stop heating, and then Add 189g of acetone, cool down to 40°C and discharge to obtain 1255g of storable vegetable oil-based polyurethane adhesive, and place it in a dry container for airtight storage. The adhesive i...
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