Alcohol-relieving and liver-protecting product made of rosemary, root of kudzu vine and lily and process
A technology of extracting rosemary, which is applied in the field of anti-alcoholic and liver-protecting products and its preparation, can solve the problems of low bioavailability, large dosage, poor effect, etc., achieve simple process, low energy consumption, and prevent human body from harming the effect of the presence of things
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Embodiment example 1
[0016] (1) 100 kg of fresh rosemary leaves, cut into sections about 2.5 cm in length, subjected to ultrasonic countercurrent extraction, the extraction solvent is 65% alcohol, the extraction temperature is 40°C, the solid-liquid ratio is 1:25, and the extract is centrifuged.
[0017] (2) Filtrate with a 50nm pore-diameter membrane. The filtrate passes through 50000 molecular weight and 10000 molecular weight, and then reaches 500 molecular weight. The unpermeated liquid is concentrated under reduced pressure until it has no alcohol smell, separated from solid and liquid, washed with appropriate amount of deionized water, and the obtained liquid is saved for future use. , and the solid was spray-dried to obtain 3.5 kilograms of rosemary fat-soluble antioxidants (crude product) with a carnosic acid content of 20-40%.
[0018] (3) The fat-soluble extract obtained in step (3) is dissolved in soybean oil and made into soft capsules, which are then treated with aluminum-plastic blist...
Embodiment example 2
[0020] (1) Fresh branches and leaves of rosemary are picked and cut, and 20% to 40% of rosemary fat-soluble extracts are produced according to steps (1) (2) in "implementation case 1".
[0021] (2) Radix Puerariae is directly crushed into coarse powder, ultrasonic countercurrent extraction, the extraction solvent is 85% edible alcohol, the solid-liquid ratio is 1:15, the extraction temperature is 65° C., the extraction time is 50 minutes, and the extract is centrifuged. The extract is filtered through a tubular membrane or a ceramic membrane (the pore size of the membrane is 30nm), the filtrate is concentrated under reduced pressure until precipitation or ethanol smell is absent, the solid and liquid are separated, and the solid is obtained by spray drying.
[0022] (3) The extract obtained in step (1) (2) is mixed uniformly with a mixer at a ratio of 7:3 to make a hard capsule preparation, which is then treated with an aluminum-plastic blister plate and packed into a warehouse...
Embodiment example 3
[0024] (1) Fresh branches and leaves of rosemary are picked and cut, and 20% to 40% of rosemary fat-soluble extracts are produced according to steps (1) (2) in "implementation case 1".
[0025] (2) Puerariae root is directly crushed into coarse powder, and the Puerariae root extract with a total flavonoid content greater than 40% is produced according to the step (2) in "Example 2".
[0026] (3) Lily raw materials are directly crushed into coarse powder, and extracted by ultrasonic countercurrent, the extraction solvent is 60% edible alcohol, the solid-liquid ratio is 1:15, the extraction temperature is 65° C., and the extraction time is 50 minutes. The extract is filtered through a tubular membrane or a ceramic membrane (with a membrane pore size of 30 nm), the filtrate is concentrated under reduced pressure and spray-dried to obtain the lily extract.
[0027] (4) Stir the extract obtained in step (1)(2)(3) evenly with a mixer at 7:2:1, add an appropriate amount of compressib...
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