Pretreatment method of wood flour suitable for plastic filling
A treatment method and pretreatment technology, which is applied in the field of wood powder pretreatment, can solve the problems of unfavorable environmental protection, waste liquid pollution, etc., and achieve the effect of improving crystallinity and good mechanical properties
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Embodiment 1
[0020] Adopt 80 mesh poplar wood flour, provided by Zhejiang Lin'an Mingzhu Bamboo and Wood Powder Co., Ltd.; PP, provided by Sinopec Shanghai Chemical Co., Ltd., brand T300, MFI=3g / 10min (2.16KG / 230 ℃), the stretching of this PP The strength is 31MPa, the bending strength is 31MPa, and the impact strength is 9KJ / m 2 . Boil the wood powder directly with an electric kettle, add wood powder and water according to the mass ratio of wood powder and water 1:8, stir until the wood powder sinks to the bottom of the pot and start heating. Boil for 10 minutes after the water boils, stop heating and suction filter while it is hot, and process the wood flour filter cake in a vacuum oven for 12 hours, and the vacuum degree of the oven is 0.09-0.1MPa. After the treatment, open the oven door to dry the wood flour to constant weight, and then sieve through 80 meshes.
[0021] Add 30phr of treated wood powder, 70phr of PP and processing aids into the HAAKE rheometer to melt and blend for 15...
Embodiment 2
[0023] Adopt 80 mesh poplar wood flour, provided by Zhejiang Linan Mingzhu Bamboo and Wood Powder Co., Ltd.; PP, provided by Sinopec Shanghai Chemical Co., Ltd., brand T300; PP-g-mah, provided by Nanjing Deba Chemical Co., Ltd., the grafting rate is about 1%. Boil the wood powder with an electric kettle, add wood powder and water according to the mass ratio of wood powder and water 1:10, stir until the wood powder sinks to the bottom of the pot and start heating. Boil for 10 minutes after the water boils, stop heating and suction filter while it is hot, and perform sauna treatment on the wood flour filter cake for 12 hours in a vacuum oven, and the vacuum degree of the oven is 0.09-0.1MPa. After the treatment, open the oven door to dry the wood flour to constant weight, and then sieve through 80 meshes.
[0024] Add 30phr of treated wood powder, 70phr of PP and 5phr of PP-g-mah into the HAAKE rheometer for melt blending for 15min at a speed of 60rpm and a blending temperature...
Embodiment 3
[0026]Adopt 80 mesh poplar wood flour, provided by Zhejiang Linan Mingzhu Bamboo and Wood Powder Co., Ltd.; PP, provided by Sinopec Shanghai Chemical Co., Ltd., brand T300; PP-g-mah, provided by Nanjing Deba Chemical Co., Ltd., the grafting rate is about 1%. Boil the wood powder with an electric kettle, add wood powder and water according to the mass ratio of wood powder and water at 1:10, boil for 15 minutes after the water boils, stop heating and suction filter while it is hot, and put the wood powder filter cake in a vacuum oven for sauna After 12 hours of treatment, the vacuum degree of the oven is at 0.09-0.1MPa. After the treatment, open the oven door to dry the wood flour to constant weight, and then sieve through 80 meshes.
[0027] Add 60phr of treated wood flour, 40phr of PP and 5phr of PP-g-mah into the HAAKE rheometer for melt blending for 15min at a speed of 60rpm and a blending temperature of 180°C; use a 25-ton flat vulcanizer to prepare composite material shee...
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