Super capacitance battery diaphragm, preparing method thereof and application thereof
A supercapacitor battery and separator technology, applied in the field of battery separators, to achieve the effects of improving ion migration capacity and exchange capacity, excellent charge retention capacity, and low internal resistance
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Embodiment 1
[0029] The fiber material is compounded according to the weight ratio, that is, polyolefin sheath-core fiber, fiber fineness 0.8D, length 38mm, content 80%; polypropylene fiber, fineness 0.8D, length 38mm, content 20%, the above-mentioned fiber is dry-processed Formed by carding process, dried in hot air at 120°C, and made into a single layer with a density of 18g / m 2 The diaphragm matrix, the density of 3 layers is 18g / m 2 The single-layer diaphragm matrix is compounded with a laminator, and adjusted to a certain thickness with a rolling mill to make a diaphragm matrix. The surface density of the diaphragm matrix is 54g / m 2 .
[0030]The diaphragm matrix is transported to the sulfonation reactor, and sulfonated with 90% concentration of gaseous sulfur trioxide, and the sulfonated matrix is transported to the alkali cleaning tank for neutralization reaction. The concentration of potassium hydroxide is 1%, and the alkali washing The speed is controlled at 20 m / min, an...
Embodiment 2
[0035] Using 100% polyolefin sheath-core fiber to make the diaphragm matrix, the fiber fineness is 0.8D, and the fiber length is 3mm to 10mm. Using wet papermaking technology, it is made into a single layer with a density of 18g after beating, molding, dehydration, and drying. / m 2 The diaphragm matrix, the density of 3 layers is 18g / m 2 The single-layer diaphragm matrix is compounded with a laminator, and adjusted to a certain thickness with a rolling mill to make a diaphragm matrix. The surface density of the diaphragm matrix is 54g / m 2 .
[0036] Then process by the sulfonation treatment of embodiment 1 and the grafting treatment mode and order of physicochemical emulsification diffusion technology, make surface density be 55g / m 2 , a supercapacitor battery diaphragm with a thickness of 0.12mm, a sulfonation degree of 0.8%, an O / C of 0.041, and a monomer grafting rate of 0.2%.
Embodiment 3
[0038] First use 100% polypropylene fiber, of which the fineness is 0.8D and the length is 38mm. It is formed by dry carding process and dried in hot air at 130°C to make a single layer with a density of 24g / m 2 the diaphragm base.
[0039] Then use 100% polyolefin sheath-core fiber, the fiber fineness is 0.8D, and the fiber length is 3mm to 10mm. Using wet papermaking technology, it is made into a single layer with a density of 23g / m after beating, molding, dehydration, and drying. 2 the diaphragm base.
[0040] Laminate the 3-layer single-layer diaphragm matrix using a laminator, wherein the middle layer is a single-layer diaphragm matrix of 100% polypropylene fiber, and the other two single layers are a single-layer diaphragm matrix of 100% polyolefin sheath-core fiber. Adjust to a certain thickness to make a diaphragm matrix, the surface density of the diaphragm matrix is 70g / m 2 .
[0041] The diaphragm matrix is transported to the sulfonation reactor, and sulfonat...
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