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Patterned transparent electrode fabrication method

A transparent electrode and patterning technology, which is applied in cable/conductor manufacturing, circuits, electrical components, etc., can solve the problems of lack of controllability of patterns and limited selection of conductive materials, so as to improve conductivity and light transmittance, and broaden the range , to ensure the effect of controllability

Active Publication Date: 2013-12-11
浙江暖科能源技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method has the characteristics of simple process and low cost, but the choice of conductive materials is limited. Only conductive materials with self-assembly properties can form patterned electrodes, and the formed patterns are also lack of controllability.

Method used

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  • Patterned transparent electrode fabrication method
  • Patterned transparent electrode fabrication method

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Experimental program
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Embodiment 1

[0018] Such as figure 1 As shown, the cellulose acetate filter membrane with a pore size of 200nm is selected as the porous filter membrane (1). The upper part of the filter membrane 1 is covered with a mask 2 and the lower part is provided with a porous sand core 3, and the mask 2 has a desired pattern Negative pattern. First, take 0.1 mg of single-walled carbon nanotube powder and add it to 200 ml of water, and add 20 g of surfactant sodium dodecyl sulfonate (SDS), and then stir to form a carbon nanotube dispersion liquid. After high-speed centrifugation at a speed of 4000 rpm and a time of 40 minutes, the supernatant is taken as the desired carbon nanotube monodisperse 4, and the concentration of the monodisperse is 0.5 wt%. Take 0.1 ml of the carbon nanotube monodispersed liquid and dilute it to 10 ml with deionized water, add the carbon nanotube monodispersed liquid 4 to the porous filter membrane 1 and filter the porous sand core 3 until the water is completely drained. ...

Embodiment 2

[0020] Preparation of graphene monodisperse solution: Take 3g of layered graphite and place it in a 250ml three-necked flask, add 70ml of concentrated sulfuric acid and 1.6g of NaNO 3 . Put the three-necked flask in an ice water bath to cool to 0°C, and then slowly add 9.0 g of potassium permanganate to keep the temperature of the mixture not exceeding 20°C. After that, the mixture was heated at 35°C, stirred and kept for 60 minutes, then 140ml of water was added dropwise within 15 minutes to cool to room temperature, and then 400ml of water and 3ml of H 2 O 2 The mixture obtained by mixing and stirring uniformly is suction filtered through a PTFE porous filter membrane with a pore size of 200 nm, and the obtained filtrate is washed with deionized water for 3 times and the collected liquid is dispersed in 200 ml of deionized water to obtain a graphene oxide dispersion. Take 100ml of the above dispersion into a 250ml three-necked flask, add 1ml of hydrazine hydrate and 5g of SDS,...

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Abstract

The invention discloses a patterned transparent electrode fabrication method. The method comprises the steps of (1) depositing a conductive nanoparticle dispersion solution on a porous filter membrane with a negative pattern mask to obtain a patterned transparent conductive film adhered on the porous filter membrane; and (2) removing the mask, transferring the patterned transparent conductive film on the porous filter membrane onto a transparent substrate, and removing the porous filter membrane to obtain the patterned transparent electrode; wherein the dispersion solution contains conductive nanoparticles 0.015wt% to 5wt%, dispersing agent 0.15wt% to 20wt%, and water in balance; and the dispersing agent is selected from arbitrary one or the combination of a surfactant, organic acid, high-molecular polysaccharide and DNA macromolecules. The method has the advantages of simple process, low cost and large material selection range, and can accurately design and control the formed pattern according to requirement.

Description

Technical field [0001] The invention relates to a method for preparing patterned transparent electrodes. Background technique [0002] Patterned transparent electrodes are widely used in fields such as display, lighting, touch control, and solar cells. At present, transparent electrode materials mainly include ITO films, conductive polymer coatings, metal nanowires, composites of metal nanoparticles and polymers, and carbon nanotube films that are sputtered onto glass or other transparent substrates by magnetron sputtering. According to the different transparent electrode materials, the current preparation methods of patterned transparent electrodes mainly include the following: 1. The most industrialized method is to etch patterns on ITO glass by photolithography, but the process is complicated. The procedures involved are cumbersome and the degree of automation in production is low. 2. In the patent document of the Lanzhou Institute of Chemical Physics, Chinese Academy of Sci...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01B13/00H01B5/14
Inventor 陈新江周红波
Owner 浙江暖科能源技术有限公司