Anti-bacterial and anti-wrinkling finishing method for cotton fabric

An anti-wrinkle finishing, cotton fabric technology, applied in fiber processing, plant fibers, textiles and papermaking, etc., can solve the problems of fabric strength loss, irritation of human skin and respiratory mucosa, carcinogenicity, etc., to achieve wrinkle recovery angle improvement, antibacterial efficiency High, formaldehyde-free effect

Active Publication Date: 2012-10-17
JIANGNAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the conventional N-methylol amide resin is usually used as the anti-wrinkle finishing agent in the prior art. Although the finishing agent has a good durable and anti-wrinkle effect, the fabrics treated by it suffer from serious loss of strength, yellowing and large amount of formaldehyde release. And other shortcomings, and in the process of storage and wearing, will continue to release formaldehyde harmful to human body, stimulate human skin and respiratory mucosa, and even cause cancer
With the improvement of living standards, people pay more attention to the functionality of clothing, and textiles that are only finished with a single antibacterial or anti-wrinkle function no longer have a competitive advantage
Patent 200510123828 discloses an anti-wrinkle finishing method for colored cotton fabrics, using N-methylolamide resin as an anti-wrinkle finishing agent; although patent 200610119085 and patent 200810184879 use polycarboxylic acid formaldehyde-free finishing agents, they are limited to a single anti-wrinkle finishing; patent 00117001 discloses a production method for antibacterial and anti-wrinkle fabrics, but the fabrics treated by this method will release free formaldehyde; Shandong Textile Science and Technology Issue 5, 2001, pages 7 to 9 disclose A polycarboxylic acid (citric acid and tartaric acid) and chitosan for anti-wrinkle and antibacterial finishing of cotton fabrics, but treating cotton fabrics with chitosan as an antibacterial agent will affect the fabric style and make the fabric surface feel rough, and the The patent has not published its antibacterial performance test effect data

Method used

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  • Anti-bacterial and anti-wrinkling finishing method for cotton fabric
  • Anti-bacterial and anti-wrinkling finishing method for cotton fabric
  • Anti-bacterial and anti-wrinkling finishing method for cotton fabric

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Dissolve sodium dihydrogen phosphate, equimolar 2,2,6,6-tetramethyl-4-piperidinol (TMP) and butane tetracarboxylic acid (BTCA) in water to form a finishing bath, in which phosphoric acid di The mass percent concentration of sodium hydrogen was 10%, and the mass percent concentration of 2,2,6,6-tetramethyl-4-piperidinol (TMP) was 1%; the untreated cotton fabric samples (purchased (Zhejiang Guandong Printing and Dyeing Garment Co., Ltd.) was immersed in the finishing bath liquid, and it was pressed and rolled on the padding car by means of two dipping and two rolling. The time was 10 minutes, and the rolling rate was 100%. ℃ pre-baking in a dryer for 10 minutes, and then baking in a baking machine at 150 ℃ for 300s; soaping the cotton fabrics after the above-mentioned baking treatment (washing the finished cotton fabrics in commercially available washing liquid for 15 minutes ), then wash and dry, and finally soak the dried cotton fabric in a sodium hypochlorite solution ...

Embodiment 2

[0020] Dissolve disodium hydrogen phosphate, equimolar 2,2,6,6-tetramethyl-4-piperidinol (TMP) and butane tetracarboxylic acid (BTCA) in water to form a finishing bath, in which hydrogen phosphate The mass percentage concentration of disodium is 5%, and the mass percentage concentration of 2,2,6,6-tetramethyl-4-piperidinol (TMP) is 5%; the untreated cotton fabric sample (same as above ) dipped in the finishing bath liquid, and rolled it on the padding car by means of double dipping and rolling for 10 minutes, and the liquid rolling rate was 100%. The cotton fabric was taken out and pre-dried in a dryer at 90°C 6min, then bake in a baking machine at 180°C for 210s; soap the cotton fabric after the above baking treatment (wash the finished cotton fabric in commercially available washing liquid for 15min), then wash and dry, Finally, soak the dried cotton fabric in a 0.5% sodium hypochlorite solution (pH 7.0) by mass percentage, take out the cotton fabric after 1 hour, and dry it...

Embodiment 3

[0022] Sodium polyphosphate, equimolar 2,2,6,6-tetramethyl-4-piperidinol (TMP) and butane tetracarboxylic acid (BTCA) are dissolved in water to form a finishing bath, in which poly The mass percentage concentration of sodium phosphate is 5%, and the mass percentage concentration of 2,2,6,6-tetramethyl-4-piperidinol (TMP) is 5%; the untreated cotton fabric sample (same as above ) dipped in the finishing bath liquid, and rolled it on the padding car by means of double dipping and rolling for 10 minutes, and the liquid rolling rate was 100%. The cotton fabric was taken out and pre-dried in a dryer at 100°C 5min, then bake in a baking machine at 180°C for 120s; soap the cotton fabric after the above baking treatment (wash the finished cotton fabric in commercially available washing liquid for 15min), then wash and dry, Finally, soak the dried cotton fabric in a calcium hypochlorite solution (pH 7) with a concentration of 0.5% by mass, take out the cotton fabric after 1 hour, and d...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention provides an anti-bacterial and anti-wrinkling finishing method for cotton fabric, comprising the following steps of: dissolving catalyst, and equimolar 2, 2, 6, 6-tetramethyl-4-pipradrol and butanetetracarboxylic acid in water, so that finishing bath foam can be formed; and soaking the cotton fabric in the finishing bath foam, treating the cotton fabric by the working procedures such as rolling and baking, soaping, washing by water, drying, halogenating and drying, wherein the catalyst is one of the sodium dihydrogen phosphate, disodium hydrogen phosphate, sodium polyphosphate and sodium hypophosphite, the halogenating treatment comprises the step of soaking the dried cotton fabric in active halogen-containing solution, and the drying temperature is 150-200DEG C. The cotton fabric which is finished by the method in an anti-bacterial and anti-wrinkling finishing way has the dual performances such as bacterial resistance and wrinkling resistance, is high in anti-bacterial efficiency, good in anti-wrinkling performance, and free from formaldehyde release.

Description

technical field [0001] The invention belongs to the technical field of textile production, and in particular relates to an antibacterial and anti-wrinkle finishing method for cotton fabrics. Background technique [0002] Cotton fabric is favored by people because of its softness, comfort, breathability, good hygroscopicity and other excellent wearing properties. However, cotton fabrics have poor resistance to microorganisms, and when worn, they will absorb the hot and humid medium emitted by the human body, providing a good environment for the reproduction of microorganisms, resulting in bad smell, even fading and discoloration of the fabric, and reduced mechanical strength; In addition, when the cotton fabric is subjected to external forces during wearing, the cellulose molecular chains or their basic structural units will undergo relative displacement, the original hydrogen bonds will be dismantled, and new hydrogen bonds will be formed. When the external force is eliminat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/236D06M101/06
Inventor 任学宏孙明明蒋之铭李蓉
Owner JIANGNAN UNIV
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