Polycrystalline silicon preparation method
A technology of polysilicon and silicon liquid, applied in chemical instruments and methods, silicon compounds, inorganic chemistry, etc., can solve the problems of poor impurity removal effect and high cost of polysilicon process, and achieve the effect of less pollution, low cost and good effect
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[0038] Example 1
[0039] (1) Weigh 0.6t of mixed slag, NaCl-KCl-SiO 2 The components by weight percentage are: NaCl is 20%, KCl is 20%, SiO 2 To 60%, put the mixed slag system into the graphite crucible of the intermediate frequency furnace to heat and melt, and keep the slag liquid temperature at 1450°C;
[0040] (2) In the process of producing silicon from the submerged arc furnace, control the quality of the silicon liquid to 1t, ensure that the mass ratio of the slag liquid to the silicon liquid is 0.6:1, and continuously inject a mixture of chlorine, oxygen and nitrogen into the bottom of the ladle. Its composition The percentage by volume is: 40% for chlorine, 20% for oxygen, 40% for nitrogen, and a ventilation flow of 5m 3 / h, pressure is 3atm, ventilation time is 1h;
[0041] (3) After the silicon output is completed, pour the slag liquid in the crucible of the intermediate frequency furnace into the ladle for refining. At the same time, turn on the ion generator to partiall...
Example Embodiment
[0052] Example 2
[0053] (1) Weigh 0.8t of mixed slag, NaCl-KCl-SiO 2 The components by weight percentage are: NaCl is 25%, KCl is 25%, SiO 2 To 50%, put the mixed slag system into the graphite crucible of the intermediate frequency furnace to heat and melt, and keep the slag liquid temperature at 1600°C;
[0054] (2) In the process of producing silicon from the submerged arc furnace, control the quality of the silicon liquid to 1t, ensure that the mass ratio of the slag liquid to the silicon liquid is 0.8, and continuously inject a mixture of chlorine, oxygen and nitrogen into the bottom of the ladle, and its composition is by volume The percentages are: 60% for chlorine, 30% for oxygen, 10% for nitrogen, and a ventilation flow of 12m 3 / h, the pressure is 9atm, the ventilation time is 3h;
[0055] (3) After the silicon output is completed, pour the slag liquid in the crucible of the intermediate frequency furnace into the ladle for refining, and turn on the ion generator at the sa...
Example Embodiment
[0066] Example 3
[0067] (1) Weigh 1t of mixed slag, NaCl-KCl-SiO 2 The components by weight percentage are: NaCl is 30%, KCl is 25%, SiO 2 45%, put the mixed slag system into the graphite crucible of the intermediate frequency furnace to heat and melt, and keep the slag liquid temperature at 1550°C;
[0068] (2) In the process of producing silicon from the submerged arc furnace, control the quality of the silicon liquid to 1t, ensure that the mass ratio of the slag liquid to the silicon liquid is 1, and continuously inject a mixture of chlorine, oxygen and nitrogen into the bottom of the ladle, and its composition is by volume The percentages are: chlorine is 50%, oxygen is 25%, nitrogen is 25%, and the ventilation flow is 10m 3 / h, pressure is 6atm, ventilation time is 2h;
[0069] (3) After the silicon is finished, pour the slag liquid in the crucible of the intermediate frequency furnace into the ladle for refining, and turn on the ion generator to partially ionize the mixed gas...
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