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Cleaning process of bismuth germanate wafer

A technology of bismuth germanate and wafer, which is applied in the directions of cleaning methods, cleaning methods and utensils, chemical instruments and methods using liquids, etc., can solve the problems of increased crystal processing cost, corrosion of bismuth germanate crystals, strong corrosion of inorganic acids, etc. , to achieve the effect of good cleaning effect, lower processing cost and less corrosive effect

Inactive Publication Date: 2013-08-07
SHANGHAI INST OF CERAMIC CHEM & TECH CHINESE ACAD OF SCI
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AI Technical Summary

Problems solved by technology

[0004] (1) Corrosion of bismuth germanate crystals: Bismuth germanate crystals are easily soluble in inorganic acids such as hydrochloric acid, sulfuric acid, and nitric acid, so corrosion of the crystals is inevitable during the process of using these inorganic acids to remove surface inorganic substances;
[0005] (2) Change the surface shape of the bismuth germanate wafer: Since the inorganic acids such as hydrochloric acid, sulfuric acid, and nitric acid in cleaning are highly corrosive to the bismuth germanate wafer, it will change the surface shape of the cut wafer, making it impossible to achieve Requirements for surface shape parameters in subsequent processes;
[0006] (3) Cause environmental pollution and increase the cost of sewage discharge: Inorganic acids such as hydrochloric acid and nitric acid are volatile and will pollute the environment; in addition, these inorganic acids are highly corrosive and require special recycling processes for treatment, which also virtually Increased cost of crystal processing

Method used

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Examples

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Effect test

Embodiment 1

[0037] Embodiment 1: a kind of cleaning process of bismuth germanate wafer

[0038] Taking the cut bismuth germanate wafer as the cleaning object, the specific operation steps are carried out in the following order:

[0039] Step 1: Preliminary cleaning to remove the obvious large-scale pollutants with weak adhesion on the surface of the wafer: Preliminary cleaning of the bismuth germanate wafer after cutting, including: first rinse the bismuth germanate wafer with secondary deionized water , and then soak in secondary deionized water at 60°C for more than 5 minutes, and finally remove the adhesive on the side with tweezers;

[0040] Step 2: Ultrasonic cleaning with aviation kerosene to remove macromolecular organic matter on the surface of the wafer: Put the bismuth germanate wafer into aviation kerosene for ultrasonic cleaning for more than 15 minutes;

[0041] The third step: ultrasonic cleaning with cleaning solution I to remove the aviation kerosene introduced in the pre...

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Abstract

The invention relates to a cleaning process of a bismuth germanate wafer. The cleaning process comprises: a preliminary cleaning step of cleaning the bismuth germanate wafer by using secondary de-ionized water to remove massive pollutants with relatively weak surface adhesive power; a second cleaning step of cleaning the bismuth germanate wafer by using aviation kerosene to remove organic greasy dirt on a surface; a third cleaning step of cleaning the bismuth germanate wafer by using a CC14 solution to further remove the organic dirt on the surface of the bismuth germanate wafer; a fourth cleaning step of cleaning the bismuth germanate wafer by using a 15%-25% propionic acid and ultrapure de-ionized water mixed solution to remove inorganic dirt on the surface; and a drying step of blow-drying the bismuth germanate wafer.

Description

technical field [0001] The invention relates to a cleaning process for a bismuth germanate wafer, belonging to the technical field of wafer processing. Background technique [0002] Bismuth germanate (Bi 4 Ge 3 o 12 ) crystal is a kind of synthetic scintillation crystal material with excellent performance. It has the advantages of high luminous efficiency, high energy resolution, stable chemical performance, matching emission spectrum and spectral response of photoelectric conversion devices, etc. It is often used as a detector for nuclear Physics, high energy physics, space science, nuclear medicine, geological survey, astrophysics and other fields. The surface of the bismuth germanate wafer after cutting usually has more pollutants such as cutting tool powder, dust in the cutting environment, bismuth germanate crystal fragments, adhesive glue, and oil stains. At present, relatively simple cleaning steps are usually used for cleaning bismuth germanate wafers after cutti...

Claims

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Application Information

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IPC IPC(8): B08B3/08B08B3/12
Inventor 卓世异黄维王乐星庄击勇陈辉
Owner SHANGHAI INST OF CERAMIC CHEM & TECH CHINESE ACAD OF SCI
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