A zirconium-doped vanadium-based oxide catalyst, preparation method and use thereof
A zirconium oxide and catalyst technology, applied in the field of zirconium-doped vanadium-tungsten-titanium oxide catalysts, can solve problems such as poor high-temperature stability, and achieve the effects of excellent high-temperature stability and excellent N2 generation selectivity.
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Embodiment 1
[0038] Dissolve 0.964g ammonium metavanadate in oxalic acid solution (mass ratio of ammonium metavanadate to oxalic acid is 1:2), make 750ml mixed solution, mix well, add 25g titanium tungsten powder (10% WO 3 -TiO 2 ), fully stirred for 1 h, and then the mixed slurry was rotatably evaporated until the water was fully volatilized, dried at 100 °C for 12 h, and finally roasted at 550 °C for 3 h to obtain 3% V 2 o 5 / 10% WO 3 -TiO 2 catalyst.
[0039] Grind and sieve the prepared catalyst, and take 40-60 mesh for later use, which is called catalyst A.
Embodiment 2
[0041] 0.964g ammonium metavanadate (NH 4 VO 3 ) was dissolved in oxalic acid solution (the mass ratio of ammonium metavanadate to oxalic acid was 1:2), and 1.74g of zirconium nitrate pentahydrate (Zr(NO 3 ) 4 ·5H 2 O), prepared into 750mL mixed solution, mix well, add 25g titanium tungsten powder (10%WO 3 -TiO 2 ), fully stirred for 1 h, and then the mixed slurry was rotatably evaporated until the water was fully volatilized, dried at 100 °C for 12 h, and finally roasted at 550 °C for 3 h to obtain 3% V 2 o 5 -2%ZrO 2 / 10% WO 3 -TiO 2 catalyst.
[0042] Grind and sieve the prepared catalyst, and take 40-60 mesh for later use, which is called catalyst B.
Embodiment 3
[0044] Other conditions are as embodiment 2 constant, change zirconium nitrate pentahydrate add-on to be 4.36g, obtain 5% V 2 o 5 -2%ZrO 2 / 10% WO 3 -TiO 2 catalyst. Grind and sieve the prepared catalyst, and take 40-60 mesh for later use, which is called catalyst C.
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