Negative electrode material for high intensity discharge lamp and manufacturing method thereof
A high-intensity discharge lamp and cathode material technology, which is applied in the field of metal material manufacturing, can solve the problems of serious discharge arc drift, reduce the life of the discharge lamp, and cumbersome steps, etc., and achieve slow grain growth, maintain shape stability, increase The effect of service life
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Embodiment 1
[0025] The manufacturing process of a discharge lamp cathode with a specification of Ф15mm is as follows
[0026] (1) Doping: Thorium nitrate, potassium aluminum silicon and blue tungsten powder are mixed and dried in the doping pot, and then enter the reduction furnace;
[0027] (2) Reduction: The reduction furnace adopts a 5-stage temperature-controlled reduction process. The five-stage temperatures are 550°C, 650°C, 750°C, 850°C, and 950°C. The holding time for each stage is 60-80min. 300-350g / boat, the reducing atmosphere is hydrogen, and the flow rate of hydrogen is 3-5m 3 / h, reduce to obtain thoriated tungsten powder containing trace potassium elements, and the powder particle size is controlled at 1.5-1.9 μm;
[0028] (4) High-energy ball milling: put the reduced doped thoriated tungsten powder into a ball milling tank lined with polyurethane for high-energy ball milling for 3-5 hours, the ball milling medium is tungsten balls, and the ball-to-material ratio is 5:1; ...
Embodiment 2
[0034] The manufacturing process of a discharge lamp cathode with a specification of Ф25mm is as follows:
[0035] (1) Doping: Thorium nitrate, potassium aluminum silicon and blue tungsten powder are mixed and dried in the doping pot, and then enter the reduction furnace;
[0036] (2) Reduction: The reduction furnace adopts a 5-stage temperature-controlled reduction process. The temperatures of the five stages are 550, 650, 750, 850, and 950°C respectively. The holding time of each stage is 60-80min. The loading capacity is 300-350g / Boat, reducing atmosphere is hydrogen, hydrogen flow rate is 3-5m 3 / h, reduce to obtain thoriated tungsten powder containing trace potassium elements, and the powder particle size is controlled at 1.5-1.9 μm;
[0037] (4) High-energy ball milling: Put the reduced doped thoriated tungsten powder into a ball milling tank lined with polyurethane for high-energy ball milling for 3-5 hours. The ball-milling medium is tungsten balls, and the ball-to-m...
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