A lithium-ion battery separator modified by polydopamine and its preparation method
A lithium-ion battery and polydopamine technology, which is applied to battery components, separators/films/diaphragms/spacers, circuits, etc., to improve ion transmission capacity, large application potential, and environmental friendliness
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Embodiment 1
[0020] Using DMF / water (volume ratio 4 / 1) as solvent, the preparation concentration is 100mmol L -1 dopamine solution, adding 0.1% by mass of graphene oxide; sodium acetate solution (1mol L -1 ) to adjust the pH to 8.5. Thickness of 10μm polyethylene diaphragm sample film 100cm 2 Immerse in 0.1kg of the above-mentioned mixed solution, at room temperature, under 10kHz, 500W ultrasound, let it stand for 2 hours, take it out, rinse it with deionized water, then repeat the test process 10 times, then place it in an argon atmosphere, and dry it at 60°C for 24 hours. That is, a modified diaphragm is obtained.
Embodiment 2
[0022] Use ethanol / water (volume ratio 1 / 4) as the solvent, and prepare the concentration at 1mmol L -1 dopamine solution, adding 10% by mass of graphene oxide; sodium acetate solution (1mol L -1 ) to adjust the pH to 8.5. Use a scraper to scrape 1kg of the mixture on 1m 2 , the surface of a polypropylene diaphragm sample with a thickness of 25 μm, and then placed in a closed container, and then the system was placed on a shaker, oscillating at a frequency of 10r / min at room temperature for 48h, then taken out, rinsed with deionized water, and then placed in a vacuum condition , dried at 100°C for 12 hours to obtain a modified separator.
Embodiment 3
[0024] Using acetone / water (volume ratio 1 / 2) as solvent, prepare a dopamine solution with a concentration of 1000mmol L-1, and add 1% graphene oxide by mass at the same time; adjust with sodium acetate solution (1mol L-1) pH to 11. Pour 5kg of mixed solution on 10m 2 , The surface of the PET membrane sample with a thickness of 100 μm, and then placed in a closed container, and then the system was placed on a shaker, oscillating at a frequency of 300r / min at room temperature, taken out after 6 hours at room temperature, rinsed with deionized water and placed in a vacuum condition 100°C for 6 hours, and then repeat the above process ten times to obtain a modified separator.
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