Silane surface treating agent and preparation method thereof
A technology of silane surface treatment and silane coupling agent, applied in the field of silane surface treatment agent and its preparation, can solve the problems of inability to form a dense film layer, decreased customer satisfaction, low solubility of magnesium carbonate, etc. The effect of saving heating energy and fast film formation
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Embodiment 1
[0057] Every 1000Kg silane surface treatment agent is made of the following raw materials:
[0058] Fluorozirconic acid 20Kg, fluotitanic acid 20 Kg, silane coupling agent (KH-560) 3 Kg, zirconium oxychloride 8 Kg, citric acid 5 Kg, water 944 Kg.
[0059] Its preparation method comprises the following steps in turn:
[0060] (1) Add water to the reactor;
[0061] (2) Add silane coupling agent into the reaction kettle and stir until the silane coupling agent is completely hydrolyzed, and the stirring time is 7-9 hours;
[0062] (3) Add fluozirconic acid and fluotitanic acid into the reaction kettle, stir evenly and make the solution clear, and the stirring time is 0.5-1.5 hours;
[0063] (4) Add zirconium oxychloride to the reaction kettle, stir evenly and make the solution clear, and the stirring time is 0.5-1.5 hours;
[0064] (5) Add citric acid into the reaction kettle, stir well and make the solution clear, and the stirring time is 20-40 minutes.
[0065] (6) Check the...
Embodiment 2
[0068] Every 1000Kg silane surface treatment agent is made of the following raw materials:
[0069] Fluorozirconic acid 20Kg, fluotitanic acid 50Kg, silane coupling agent (KH-560) 3Kg, zirconium oxychloride 8Kg, citric acid 5Kg, water 914Kg.
[0070] The preparation method is the same as in Example 1.
[0071]
Embodiment 3
[0073] Every 1000Kg silane surface treatment agent is made of the following raw materials:
[0074] Fluorozirconic acid 40Kg, fluotitanic acid 30Kg, silane coupling agent (KH-560) 5Kg, zirconium oxychloride 10Kg, citric acid 7Kg, water 908Kg.
[0075] The preparation method is the same as in Example 1.
[0076]
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