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195results about "Alkali metal nitrates" patented technology

Complete equipment for stainless steel pickling wastewater treatment and resource recycling and treatment process

Complete equipment for stainless steel pickling wastewater treatment and resource recycling and a treatment process are disclosed. A pretreatment section, a membrane treatment section and a quality-based crystallization section are involved. The invention is characterized in that a storage regulating basin, a neutralization-oxidation reaction tank, a flocculent precipitation tank, a filter, an ultrafiltration and reverse osmosis system, a membrane concentration system and an evaporation and concentration and quality-based crystallization system are mutually connected end to end through pipelines. Each dosage device is respectively arranged on corresponding section. According to the order of the pretreatment section, the membrane treatment section and the quality-based crystallization section, thirteen steps are included for the operation. By the treatment process of chemical reactive precipitation, membrane separation concentration and evaporation and quality-based crystallization, various acid wastewaters mainly containing acid and inorganic salt can be treated to realize recycling of wastewater. After crystallization of salt, sodium sulfate (and sodium chloride), sodium nitrate, sodium fluoride and other products can be recycled, and zero-discharge resource utilization of stainless steel pickling wastewater is realized. Meanwhile, system sludge yield is greatly reduced such that the burden of sludge treatment is decreased.
Owner:MAIWANG INT BUSINESS SHANGHAI

System and technology for recovering sodium nitrate from tin-containing waste liquid treatment tail water

The invention relates to a system and a technology for recovering sodium nitrate from tin-containing waste liquid treatment tail water. The system for recovering sodium nitrate from tin-containing waste liquid treatment tail water comprises a waste water storage pool, a purification refining device, a multi-effect evaporator, a filter, a crystallization device, a centrifugal machine and a drying machine. The technology for recovering sodium nitrate from tin-containing waste liquid treatment tail water comprises the following steps of collecting tin-containing waste liquid treatment tail water, storing the collected tin-containing waste liquid treatment tail water in the waste water storage pool, feeding the tin-containing waste liquid treatment tail water in the waste water storage pool into the purification refining device to carry out purification refining, feeding the tin-containing waste liquid treatment tail water subjected to purification refining into the multi-effect evaporator, feeding steam into the multi-effect evaporator to carry out circulation evaporation, feeding the steam obtained by the previous step into the filter to carry out heat filtration, feeding the filtrate into the crystallization device to carry out crystallization to obtain crystals, carrying out centrifugation of the obtained crystals by the centrifugal machine to obtain solid slag and a mother solution, transferring the solid slag to the drying machine to carry out drying to obtain a sodium nitrate finished product, and feeding the mother solution back to the waste water storage pool for recycle. The system for recovering sodium nitrate from tin-containing waste liquid treatment tail water has the advantages of relatively low recovery cost, simple and convenient operation management, long-term and stable operation and no discharge of pollutants.
Owner:无锡金品环境技术有限公司

Zero-emission sewage reutilization device and method

The invention relates to the technical field of zero-emission sewage reutilization and provides a zero-emission sewage reutilization device. A zero-emission sewage reutilization method sequentially comprises steps as follows: miscellaneous salt is subjected to coagulative sedimentation, sodium carbonate is added and calcium carbonate precipitates are obtained; caustic soda is added, and magnesium hydroxide is obtained; membrane filtration is performed, the pH value is regulated, ion exchange softening, advanced oxidation, biochemical treatment with a biological membrane are performed, filtration with a membrane filter and nanofiltration are performed, lime milk is added to interception water obtained through nanofiltration, calcium sulfate is obtained, a supernatant flows back to a miscellaneous salt sedimentation basin, nanofiltration permeate water is concentrated through a reverse osmosis separator A and then is concentrated by a brine concentrator, fresh water produced by the brine concentrator is concentrated by a reverse osmosis concentrator B and flows back to the brine concentrator, concentrated water produced by the brine concentrator enters an crystallizing evaporator and is subjected to hot separation and cold separation, sodium chloride and sodium nitrate are obtained respectively, most crystallization mother liquor is subjected to refluxing treatment, and a small part of crystallization mother liquor is dried; reverse osmosis produced water and distilled water are reused. According to the invention, commercial calcium carbonate, magnesium hydroxide, calcium sulfate, sodium chloride, sodium nitrate salts and high-quality reused water are recycled, emission of solid waste is small, and the operating cost is low.
Owner:GELANTE ENVIRONMENTAL PROTECTION ENG BEIJING CO LTD

Method for preparing water soluble sylvite

The invention discloses a method for preparing water soluble sylvite. The method includes the steps that A, inorganic base salt and smashed potassium-rich rock are mixed to obtain a first mixture, acid radical negative ions of the inorganic base salt correspond to negative ions of the water soluble sylvite, and the potassium-rich rock is the silicate mineral with the mass percent larger than or equal to 8% in terms of K2O; B, the first mixture is heated to be at the temperature smaller than or equal to 300 DEG C and melted, and a second mixture is obtained; C, the second mixture is heated to be at the temperature of 500 DEG C to 1,200 DEG C in a microwave mode, the temperature is kept for 10 min to 2 h, and a third mixture is obtained; D, the third mixture is cooled to be at the temperature of 80 DEG C to 120 DEG C, then water is led into the cooled third mixture, a fourth mixture is obtained, the temperature of the fourth mixture is kept for 6 h to 48 h at the temperature of 50 DEG C to 90 DEG C, solid-liquid separation is carried out, and then first filtered liquid is obtained; E, the first filtered liquid is concentrated and cooled, and the soluble sylvite is separated out. According to the preparing method, the potassium-rich rock serves as a raw material, a water solution of the soluble sylvite is obtained through two-time extracting, the technology is simple, the preparing cost is low, and the technology is safe.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI

Method for recycling dimethyl sulfoxide waste residue through multi-stage extraction

The invention provides a method for recycling dimethyl sulfoxide waste residue through multi-stage extraction. The first-stage extraction comprises the steps of separating dimethyl sulfone and dimethyl sulfoxide by using an extracting agent (benzene) and respectively recycling the extracting agent (benzene), dimethyl sulfoxide and dimethyl sulfone products by using a distilling and condensing way; the second-stage extraction comprises the steps of separating benzene residual liquor containing dimethyl sulfone and dimethyl sulfoxide out of the solid phase (obtained after the first-stage extraction) in the presence of an extracting agent (methanol), respectively recycling the extracting agent (methanol) and the benzene residual liquor by using a distilling and condensing method and returning the benzene residual liquor to a former distillation tower; the solid phase in the second-sage extraction is dissolved by using water, air or oxidant is introduced to oxidize sodium nitrite into sodium nitrate, and then sodium nitrate is evaporated and crystallized to extract inorganic components. The treatment method disclosed by the invention is simple and safe in process, low in evaporation temperature, operated at ordinary pressure, easy to implement and low in operation cost, the whole course is of close circulation, components of the waste residue are completely recycled, the recycling efficiency is high, the secondary pollution of waste is avoided, pollution problem caused by the dimethyl sulfoxide production waste residue can be solved, and a certain economic value is created.
Owner:HUBEI UNIV

Equipment special for producing bulk wet salt by using sodium sulfate type brine

The invention relates to equipment special for producing bulk wet salt by using sodium sulfate type brine. The equipment comprises a multi-stage preheater, an autoclave and a vapor compression system; a salt slurry outlet of the autoclave is communicated with salt centrifugal dehydration equipment; the equipment also comprises an energy saving device, a salt-making vaporizing tank and a nitre-making vaporizing tank which are communicated through a pipeline; a brine outlet of the autoclave is communicated with a brine inlet of the energy saving device; a brine outlet of the energy saving device is communicated with a brine inlet of the salt-making vaporizing tank; a brine outlet of the salt-making vaporizing tank is communicated with a brine inlet of the nitre-making vaporizing tank; a salt slurry outlet of the salt-making vaporizing tank is communicated with the salt centrifugal dehydration equipment; a nitre slurry outlet of the nitre-making vaporizing tank is communicated with nitre centrifugal dehydration equipment; and a brine outlet of the nitre-making vaporizing tank is communicated with the brine inlet of the energy saving device. The equipment special for producing the bulk wet salt by using the sodium sulfate type brine is provided with the salt-making vaporizing tank and the nitre-making vaporizing tank for salt-nitre separation, the salt-making and nitre-making efficiency is improved, and the energy saving device is adopted for recycling heat.
Owner:CHINASALT JINTAN
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