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A mold and method for producing copper-zinc-tin rotating target

A rotating target, copper-zinc-tin technology, which is applied in the direction of manufacturing tools, metal material coating process, ion implantation plating, etc., can solve the problem of not seeing the rotating copper-zinc-tin target, etc., and achieve good composition distribution uniformity, The effect of fine crystal grains and high purity

Active Publication Date: 2016-04-06
无锡鑫聚电子科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, a large number of rotating copper-zinc-tin targets is an inevitable trend in the development of copper-zinc-tin-sulfur thin-film solar cells, and there are no reports on the production of rotating copper-zinc-tin target technology.

Method used

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  • A mold and method for producing copper-zinc-tin rotating target
  • A mold and method for producing copper-zinc-tin rotating target
  • A mold and method for producing copper-zinc-tin rotating target

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Such as figure 1 As shown, a mold for producing a copper-zinc-tin rotating target includes a casting port 1, which is connected to a mold jacket 2; a liner 4 is arranged inside the mold jacket 2, and a An annular cavity 3; the bottom of the mold jacket 2 and the liner 4 are sealed with a bottom sealing ring 5.

[0019] The casting port 1 communicates with the annular cavity 3 through a flow pipe, and the flow pipe is inclined toward the interior of the annular cavity 3 . A layer of isolation layer is coated on the inner wall of the jacket 2, and the isolation layer is DY08 paint.

Embodiment 2

[0021] A method for producing a copper-zinc-tin rotating target, the steps are:

[0022] (1) Melting: Take raw materials according to the copper: zinc: tin molar ratio of 1.5:0.7:0.8; open the vacuum induction melting furnace, evacuate to 0.01Pa, pass nitrogen, and when the pressure reaches 0.08MPa, evacuate again to 0.01Pa; Put raw tin into the smelting furnace, smelt until completely melted at 250°C, control the temperature at 250°C, put in copper, continue smelting until completely melted, raise the temperature to 670°C, refine for 35 minutes, and finally put in zinc, control the temperature not to exceed 700°C for rapid melting , after melting completely, refining at 680°C for 12 minutes to obtain casting solution;

[0023] (2) Casting: Take the mold for producing copper-zinc-tin rotating target, dry it at 200°C, and preheat it to 600°C, pour the casting liquid obtained in step (1) into the mold; Cavity 3, the paint coated on the inner wall of jacket 2 prevents the mold f...

Embodiment 3

[0028] A method for producing a copper-zinc-tin rotating target, the steps are:

[0029] (1) Smelting: Take raw materials according to the molar ratio of copper: zinc: tin: 2.3:1.2:1.1; open the vacuum induction melting furnace, evacuate to 1Pa, pass nitrogen, and when the pressure reaches 0.1MPa, evacuate to 1Pa again; Put the raw material tin into the furnace, smelt it at 270°C until it is completely melted, control the temperature at 300°C, put in copper, continue to smelt it until it is completely melted, raise the temperature to 750°C, refine it for 25 minutes, and finally put in zinc, control the temperature not to exceed 700°C for rapid melting, all After melting, refining at 690°C for 8 minutes to obtain casting solution;

[0030] (2) Casting: Take the mold for producing copper-zinc-tin rotating target, dry it at 450°C, and preheat it to 600°C, pour the casting solution obtained in step (1) into the mold; Cavity 3, the paint coated on the inner wall of jacket 2 preven...

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Abstract

The invention relates to a production mold and production method of a copper-zinc-tin rotary target, belonging to the technical field of functional materials. The method comprises the following steps: smelting raw materials to obtain a casting solution, casting into the mold for producing the copper-zinc-tin rotary target, cooling, and stripping to obtain the copper-zinc-tin rotary target. The target has the advantages of high density, high purity, favorable component distribution uniformity and small crystal grains; and the method has the advantages of simple preparation technique and low cost, and can be used for large-scale industrial production.

Description

technical field [0001] The invention relates to a production mold for a copper-zinc-tin rotating target and a production method thereof, belonging to the technical field of functional materials. Background technique [0002] With the increasing shortage and reduction of world energy and the enhancement of people's awareness of environmental protection, the research and application of thin-film solar cells has become a research hotspot all over the world. Among them, copper-zinc-tin-sulfur thin-film solar cells are attracting more and more attention due to their high conversion efficiency, low production cost, no performance degradation and environmental friendliness. [0003] Cu 2 ZnSnS 4 (referred to as CZTS) thin-film solar cell as a new type of thin-film solar cell has a multi-layer film structure, its main structure is metal gate Al, window layer n-ZnO: Al, buffer layer CdS, absorption layer CZTS, back electrode molybdenum, Soda lime glass substrate SLG, etc. [0004...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/34B22C9/00C22C9/00C22C1/02
Inventor 胡习光秦国强常金永张志祥
Owner 无锡鑫聚电子科技有限公司