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Butyl rubber composition, preparation method and method for preparing pressure hose

A technology of butyl rubber and pressure-resistant hoses, which is applied in the direction of hoses, pipes, mechanical equipment, etc., can solve the problems of easy peeling, poor bonding strength, and poor pressure resistance of hoses, and achieve good low temperature resistance and mechanical properties performance, good bonding performance, and the effect of improving bonding strength

Active Publication Date: 2014-10-08
AEROSPACE RES INST OF MATERIAL & PROCESSING TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The pressure resistance performance depends on the high-strength braided jacket and the adhesion between the braided jacket and the inner rubber. If the bonding strength between the outer jacket and the inner rubber is high, the pressure resistance of the hose will be good. If the adhesive strength is poor, the hose will withstand pressure. poor performance
The air tightness mainly depends on the inner lining layer, so the inner lining layer material can choose butyl rubber with good air permeability resistance and low cost as the base compound, but because butyl rubber contains very few cross-linking double bonds, The bonding strength between the lining rubber material mainly made of butyl rubber and the braided layer jacket is poor, and its T-peel strength is less than 1.5N cm, which is easy to peel off, resulting in wrinkles on the surface of the hose and poor appearance quality, which affects the softness of the hose. The pressure resistance of the tube is high, and the service life is short; in addition, if the bonding force between the rubber lining and the braided outer tube blank is small, the rubber lining tube is easy to peel off and damage during the folding process of the hose, and cannot be repaired, resulting in scrap
[0004] Therefore, there is an urgent need to develop a lining rubber material with high strength combined with the braided jacket to solve the problem of bonding strength between the braided jacket and the rubber lining of the high-pressure airtight foldable rubber hose, thereby improving the pressure resistance and serviceability of the hose. life

Method used

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  • Butyl rubber composition, preparation method and method for preparing pressure hose
  • Butyl rubber composition, preparation method and method for preparing pressure hose
  • Butyl rubber composition, preparation method and method for preparing pressure hose

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1~6

[0032] According to the mixing ratio in Table 1, use an open mill to mix the rubber materials. First, put the butyl rubber and neoprene raw rubber on the rollers. After the rubber materials are completely covered with the rollers, add calcium carbonate and stearin. Acid and lithopone, mixing 120~300 seconds (embodiment 1~2 mixing 180 seconds; Embodiment 3~4 mixing 210 seconds; Embodiment 5~6 mixing 250 seconds;), mixing time according to adding Whether the compounding agent is mixed or not shall prevail; to adjust the roller distance, white carbon black may be added according to the principle of a small amount of multiple batches, and the mixing time is 120 to 240 seconds (Examples 1 to 2 are mixed for 180 seconds; Examples 3 to 4 are mixed Refining for 150 seconds; Example 5-6 mixing for 200 seconds;); then add magnesium oxide, zinc oxide, anti-aging agent, and plasticizer (half of the total mass), and mix for 120-360 seconds according to the dispersed state of the compounding...

Embodiment 1

[0039] The hardness of the vulcanized rubber of the lining rubber butyl rubber composition is 55, the tensile strength is 6.6MPa, the elongation at break is 701%, and the brittle temperature reaches -50°C;

[0040] The T-peel strength of the braided jacket and the rubber lining is 9.36N cm;

[0041] The hydraulic burst pressure of the pressure hose is 4.12MPa.

Embodiment 2

[0043] The hardness of the vulcanized rubber of the lining rubber butyl rubber composition is 48, the tensile strength is 5.7MPa, the elongation at break is 721%, and the brittle temperature reaches -40°C;

[0044] The T-peel strength of the braided jacket and the rubber lining is 3.70N cm;

[0045] The hydraulic burst pressure of the pressure hose is 3.28MPa.

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Abstract

The invention relates to a butyl rubber composition, a preparation method and a method for preparing a pressure hose. The preparation method comprises: (1) putting butyl rubber and chloroprene rubber on a roller, after the roller is completely coated, adding calcium carbonate, stearic acid and lithopone, performing mixing, then adding white carbon black in batches, performing mixing, then adding magnesium oxide, zinc oxide, an anti-ageing agent and a half amount of a plasticizer, performing mixing, then adding a coupling agent, paraffin and a tackifier, and performing mixing and thin passing; and (2) performing straining on mixed rubber by using a straining machine, putting on a roller again, then adding a vulcanizing agent, an auxiliary vulcanizing agent and the other half amount of the plasticizer, and performing mixing and thin passing. The prepared butyl rubber composition has excellent performance. By employing the butyl rubber composition for preparing a lining rubber pipe, the caking strength between a woven layer and a lining layer of a pressure-resistant airtight foldable hose is substantially improved, and the pressure-resistant performance and the airtightness of the hose are substantially improved.

Description

technical field [0001] The invention belongs to the field of polymer material processing, and relates to a butyl rubber composition, a preparation method and a method for preparing a pressure-resistant hose. Background technique [0002] Usually, the conveying hoses used in fire hoses or other special fields are composed of reinforced material woven tube blanks and anti-leakage lining materials, which require certain air permeability resistance, high pressure resistance, high temperature resistance, and weather resistance. The outer layer is mostly a cylindrical fabric woven with high-strength synthetic fibers or metal filaments, and the inner lining is mostly made of anti-leakage rubber or latex material. Latex-lined hoses have poor flexibility and are not easy to fold; rubber-lined hoses are widely used because of their good air tightness, lightness in use, easy operation, good flexibility and foldability within a certain temperature range. [0003] With the higher requir...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/22C08L11/00C08K13/02C08K3/26C08K3/36C08K3/30C08K5/09C08K3/22C08K5/01F16L11/04B29B7/56
CPCC08L23/22B29B7/56C08L2205/035C08L2203/18C08L11/00C08L91/06C08L61/14C08K13/02C08K2003/265C08K3/36C08K2003/3045C08K5/09C08K2003/222B29B7/7495
Inventor 刘小艳吴福迪张继华赵云峰王帮武王立峰皂伟涛伍芃李杰朱军
Owner AEROSPACE RES INST OF MATERIAL & PROCESSING TECH
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