A kind of power battery ceramic sealed connector and preparation method thereof
A ceramic sealing and power battery technology, which is applied in the field of ceramic metal materials, can solve the problems that the battery cannot be connected as one, the sealing strength is high, and the metal material has no insulation performance, so as to broaden the welding production and use process conditions and improve the bending resistance Strength and tensile strength, effect of high-tight welded connection
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Embodiment 1
[0025] (1) Ingredients synthesis: Weigh Al 2 o : 20 parts and ZrO 2 1 part, modifier MgO is 0.21 part, sintering aid CaCO 3 0.84 parts, mix the ingredients and put them into a baking oven for baking. The baking temperature is 150°C and the baking time is 15 hours. Then put them into a ball mill for ball milling for 24 hours to obtain uniformly refined mixed raw materials. The particle size Reach 3-3.5μm;
[0026] (2) Pre-burning: Pre-burn in the air at a temperature of 4°C per minute to 1150°C for 2 hours, then cool down with the furnace, then crush the resulting mixed raw materials, perform a second ball mill, pass through a 80-mesh sieve and then dry , making Al 2 o 3 Powder;
[0027] (3) Granulation: Al 2 o 3 Add 10% polyvinyl alcohol to the powder, and use a granulator to granulate;
[0028] (4) Dry pressing: use a press to perform dry pressing under 6MPa to obtain ceramic blanks;
[0029] (5) Sintering: Sinter the ceramic blank, control the temperature at 37°C-...
Embodiment 2
[0036] (1) Ingredients synthesis: Weigh Al 2 o : 40 parts and ZrO 2 2 parts, modifier MgO is 0.63 parts, sintering aid CaCO 3 1.89 parts, mix the ingredients and put them in a baking oven for baking. The baking temperature is 150°C and the baking time is 15 hours. Then put them into a ball mill for ball milling for 24 hours to obtain uniformly refined mixed raw materials. The particle size Reach 3-3.5μm;
[0037] (2) Pre-burning: Pre-burn in the air at a temperature of 4°C per minute to 1150°C for 2 hours, then cool down with the furnace, then crush the resulting mixed raw materials, perform a second ball mill, pass through a 80-mesh sieve and then dry , making Al 2 o 3 Powder;
[0038] (3) Granulation: Al 2 o 3 Add 10% polyvinyl alcohol to the powder, and use a granulator to granulate;
[0039] (4) Dry pressing: use a press to perform dry pressing under 6MPa to obtain ceramic blanks;
[0040] (5) Sintering: Sinter the ceramic blank, control the temperature at 37°C-...
Embodiment 3
[0047] (1) Ingredients synthesis: Weigh Al 2 o : 80 parts and ZrO 2 4 parts, modifier MgO is 1.68 parts, sintering aid CaCO 3 4.2 parts, mix the ingredients and put them in a baking oven for baking. The baking temperature is 150°C and the baking time is 15 hours. Then put them into a ball mill for ball milling for 24 hours to obtain uniformly refined mixed raw materials. The particle size Reach 3-3.5μm;
[0048] (2) Pre-burning: Pre-burn in the air at a temperature of 4°C per minute to 1150°C for 2 hours, then cool down with the furnace, then crush the resulting mixed raw materials, perform a second ball mill, pass through a 80-mesh sieve and then dry , making Al 2 o 3 Powder;
[0049] (3) Granulation: Al 2 o 3 Add 10% polyvinyl alcohol to the powder, and use a granulator to granulate;
[0050] (4) Dry pressing: use a press to perform dry pressing under 6MPa to obtain ceramic blanks;
[0051] (5) Sintering: Sinter the ceramic blank, control the temperature at 37°C-3...
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