Production method for preparing ammonium dihydrogen phosphate and byproduct special fertilizer for radix scutellariae
A technology of ammonium dihydrogen phosphate and ammonium dihydrogen phosphate, which is applied in the direction of phosphate, phosphorus oxyacid, application, etc., can solve the problems of reducing the output and quality of Huangling, difficulty in meeting industrial needs, and impact on purity, and achieves significant Environmental protection value and economic benefits, increase product added value, output and quality improvement effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0046] A kind of production method of preparing ammonium dihydrogen phosphate by-product Huang Ling special fertilizer, comprises the following steps:
[0047] (1) Preparation and mixing of raw materials: Put phosphoric acid and urea in a stirred reactor at a molar ratio of 1.5:1, at a temperature of 90°C, and control the stirring speed of the stirred tank at 180r / min to stir and mix for 1 hour to obtain an intermediate material pulp;
[0048] (2) Preparation of ammonium dihydrogen phosphate: Ammonia gas is passed into the intermediate slurry obtained in step 1), and the temperature in the reactor is controlled to be 70°C, and the stirring speed is 60r / min, and the stirring reaction is 30min, and the reaction ends PH value is 4.2, obtains the slurry containing ammonium dihydrogen phosphate product;
[0049] (3) Cyclic crystallization and filtration: place the slurry containing ammonium dihydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a temper...
Embodiment 2
[0056] A kind of production method of preparing ammonium dihydrogen phosphate by-product Huang Ling special fertilizer, comprises the following steps:
[0057] (1) Preparation and mixing of raw materials: Put phosphoric acid and urea in a stirred reactor at a molar ratio of 1.7:1, at a temperature of 140°C, and control the stirring speed of the stirred tank at 200r / min to stir and mix for 3 hours to obtain an intermediate material pulp;
[0058] (2) Preparation of ammonium dihydrogen phosphate: Ammonia gas is passed into the intermediate slurry obtained in step 1), and the temperature in the reactor is controlled to be 80°C. According to the stirring speed of 80r / min, the stirring reaction is 40min, and the reaction ends PH value is 4.6, obtains the slurry containing ammonium dihydrogen phosphate product;
[0059] (3) Cyclic crystallization and filtration: place the slurry containing ammonium dihydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a...
Embodiment 3
[0066] A kind of production method of preparing ammonium dihydrogen phosphate by-product Huang Ling special fertilizer, comprises the following steps:
[0067] (1) Preparation and mixing of raw materials: Put phosphoric acid and urea in a stirred reactor at a molar ratio of 1.6:1, at a temperature of 125°C, and control the stirring speed of the stirred tank at 190r / min to stir and mix for 2 hours to obtain an intermediate material pulp;
[0068] (2) Preparation of ammonium dihydrogen phosphate: Ammonia gas is passed into the intermediate slurry obtained in step 1), and the temperature in the reactor is controlled to be 75°C. According to the stirring speed of 70r / min, the stirring reaction is 35min, and the reaction ends PH value is 4.4, obtains the slurry containing ammonium dihydrogen phosphate product;
[0069] (3) Cyclic crystallization and filtration: place the slurry containing ammonium dihydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com