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Powder metallurgy lubricant and preparation method thereof for stainless steel

A powder metallurgy and lubricant technology, applied in the field of powder metallurgy lubricant for stainless steel and its preparation, can solve the problems of unsatisfactory improvement of powder metallurgy products, unstable filling of mixed powder, great influence on green strength of products, etc. The effect of blank strength and surface finish, improving surface finish, yield and quality

Inactive Publication Date: 2015-03-04
SUZHOU NETABHAPE COMPOSITE MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But these lubricants have more or less problems
Micro-powdered wax products have better volatilization performance during use, but the improvement of powder metallurgy products in terms of flow rate and compaction performance of the product is not ideal, and sometimes it will reduce the flow performance of the powder, resulting in unstable filling of the mixed powder
Zinc stearate and lithium stearate are commonly used lubricants, but due to the chemical properties of the product itself, a large amount of carbon will remain on the surface of the product after sintering, and the zinc oxide after sintering will also cause pollution to the sintering furnace, affecting the product The green strength of the
Although the imported Heganus Kenolube P11 has obvious advantages in comprehensive performance, it is only limited to the high powder filling height of some products. For large-sized products, it will still affect the release of the product, and Kenolube P11 contains metal zinc. Therefore, there will still be some carbon deposits on the surface during the sintering process, which will pollute the furnace at the same time.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Powder metallurgy lubricant for stainless steel, the raw materials include in parts by weight: 3 parts of polyethylene vinyl acetate, 2 parts of graphite, 1 part of zinc stearate, 4 parts of vinyl bis stearamide, 5 parts of paraffin wax, 1 part of octadecylamine 2 parts, 2 parts of sodium petroleum sulfonate, 3 parts of sodium benzoate, 5 parts of thionyl octyl zinc, 3 parts of tributylamine octanoate, 2 parts of amino silicone oil, 1 part of alkyl diphenylamine, 2 parts of oleic acid amide.

[0019] Above-mentioned graphite particle size is 100 orders, and paraffin is liquid paraffin.

[0020] The preparation method of the above-mentioned powder metallurgy lubricant for stainless steel comprises the following steps:

[0021] Step 1: Mix polyethylene vinyl acetate, graphite, zinc stearate, vinylbisstearamide and paraffin, heat at a constant temperature of 130°C for 40 minutes, and cool to room temperature to obtain mixture I;

[0022] Step 2, add octadecylamine, sodium...

Embodiment 2

[0024] Powder metallurgy lubricant for stainless steel, the raw materials include in parts by weight: 4 parts of polyethylene vinyl acetate, 3 parts of graphite, 2 parts of zinc stearate, 6 parts of vinylbisstearamide, 6 parts of paraffin wax, 1 part of octadecylamine 3 parts, 3 parts of sodium petroleum sulfonate, 5 parts of sodium benzoate, 6 parts of thionyl octyl zinc, 4 parts of tributylamine octanoate, 3 parts of amino silicone oil, 2 parts of alkyl diphenylamine, 4 parts of oleic acid amide.

[0025] Above-mentioned graphite particle size is 120 orders, and paraffin is liquid paraffin.

[0026] The preparation method of the above-mentioned powder metallurgy lubricant for stainless steel comprises the following steps:

[0027] Step 1: Mix polyethylene vinyl acetate, graphite, zinc stearate, vinylbisstearamide and paraffin, heat at a constant temperature of 160°C for 20 minutes, and cool to room temperature to obtain mixture I;

[0028] Step 2, add octadecylamine, sodium...

Embodiment 3

[0030] Powder metallurgy lubricant for stainless steel, the raw materials include in parts by weight: 5 parts of polyethylene vinyl acetate, 4 parts of graphite, 2 parts of zinc stearate, 9 parts of vinylbisstearamide, 7 parts of paraffin, 5 parts of octadecylamine 7 parts, 7 parts of sodium petroleum sulfonate, 5 parts of sodium benzoate, 9 parts of thionyl octyl zinc, 6 parts of tributylamine octanoate, 5 parts of amino silicone oil, 2 parts of alkyl diphenylamine, 7 parts of oleic acid amide.

[0031] Above-mentioned graphite particle size is 140 orders, and paraffin is liquid paraffin.

[0032] The preparation method of the above-mentioned powder metallurgy lubricant for stainless steel comprises the following steps:

[0033] Step 1: Mix polyethylene vinyl acetate, graphite, zinc stearate, vinylbisstearamide and paraffin, heat at a constant temperature of 140°C for 30 minutes, and cool to room temperature to obtain mixture I;

[0034] Step 2, add octadecylamine, sodium pe...

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Abstract

The invention provides a powder metallurgy lubricant and a preparation method thereof for stainless steel. The lubricant comprises the raw materials of polyethylene vinyl acetate, graphite, zinc stearate, vinyl-bis-stearamide, paraffin wax, octadecyl amine, petroleum sodium sulfonate, sodium benzoate, zinc butyl octyl phosphate, octoate tributylamine, amino silicone oil, alkyl diphenylamine and oleamide. The preparation method comprises the following steps: firstly mixing the polyethylene vinyl acetate, graphite, zinc stearate, vinyl-bis-stearamide and paraffin wax, and heating at a constant temperature to obtain a mixture I; then adding the remaining raw materials into the mixture I, cooling to the room temperature, and then grinding, crushing, and sieving to obtain the lubricant. The lubricant provided by the invention can improve the green compact strength and finish surface, greatly prolongs the service life of a mould, and improves the productivity, the yield and the quality of a powder metallurgy stainless steel product.

Description

technical field [0001] The invention belongs to the technical field of powder metallurgy material additives, and in particular relates to a powder metallurgy lubricant for stainless steel and a preparation method thereof. Background technique [0002] With the continuous development of the economy, stainless steel products are used more and more widely. As a near net shape technology, powder metallurgy stainless steel has great advantages in the production of stainless steel parts with expensive raw materials. Moreover, most of the stainless steel is austenitic stainless steel or ferritic stainless steel, which leads to high processing costs due to poor processing performance. Powder metallurgy stainless steel products can avoid or reduce the amount of machining, and have more advantages in cost. But also because stainless steel belongs to high-alloy steel, the particle hardness of stainless steel powder still has Hv180-210 due to solid solution strengthening after eliminat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/04B22F1/00C10N40/24C10N30/06C10N30/12C10N40/36
Inventor 刘莉王爽刘晓东
Owner SUZHOU NETABHAPE COMPOSITE MATERIALS
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