Preparation method of hydrophobic nano-modified resin composite coating for LED substrate
A LED substrate, hydrophobic nano technology, applied in the field of coatings, can solve the problems of no thermal conductivity, small thermal conductivity, and inability to achieve smooth heat dissipation channels
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[0013] The present invention is further described below by example.
[0014] The preparation method of the nano-modified resin composite coating that is used for LED substrate among the present invention, comprises the steps:
[0015] (1) At a stirring rate of 800 to 1000r / min, 20 to 30 parts by mass of nano-α-Al 2 o 3 and 55-70 parts by mass of butanol are added to the disperser to disperse evenly; then HCl is added to adjust the concentration of hydrogen ions in the system at 10 -3 ~10 -4 M, then add 10-15 parts by mass of silane coupling agent KH560, and age at 50°C for 24 hours to obtain nano-α-Al surface-modified by KH560 2 o 3 Sol.
[0016] (2) Add 20-30 parts by mass of tridecafluorooctyltriethoxysilane to 57-74 parts by mass of n-butanol, add 1-3 parts by mass of formic acid and mix well, add 5-10 parts by mass of deionized water, Aged at 60°C for 48 hours to obtain a fluorosilane oligomer sol.
[0017] (3) Utilize the L-H type rotary evaporator to modify the α-...
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