High-strength gel for snubbing operation and preparation method of high-strength gel
A high-strength, jelly-gel technology is used in the application field of chemical agents in petroleum drilling and completion engineering, which can solve the problem that the bridge plug rubber core cannot be well adapted to different pipe diameters, the operator has high technical requirements, and restricts the snubbing operation. Development and other issues, to achieve the effects of controllable glue forming time, broadening the scope of application, and controllable body strength
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Embodiment 1
[0028] A kind of high-strength jelly for snubbing operation provided by the present invention, wherein the weight percent of each component is: cornstarch 3%, oxidation-reduction initiator ammonium persulfate 0.03%, sodium bisulfite 0.01%, cross Linking agent A melamine 10%, crosslinking agent B formaldehyde aqueous solution 7.5%, initiator monomer acrylamide 10%, curing agent urotropine 0.02%, and the rest is water.
[0029] Under stirring conditions, gelatinize 2g of corn starch in water at 75°C for 1 hour in a container, adjust its pH value to 10 after starch gelatinization, adjust its temperature to 80°C, and keep it at a constant temperature for 60 minutes, then proceed according to the proportion Add ammonium persulfate, sodium bisulfite, melamine, formaldehyde solution, acrylamide and urotropine and stir evenly, then continue to stand at the above temperature for 60 minutes to form a gel.
[0030] The obtained colloid has a viscosity of 30000mPa.s and a maximum plugging...
Embodiment 2
[0032] A kind of high-strength jelly for snubbing operation provided by the present invention, wherein the weight percent of each component is: cornstarch 3%, water-soluble oxidation-reduction gel initiator potassium persulfate 0.3% and sodium bisulfite 0.2%, cross-linking agent A melamine 10%, cross-linking agent B formaldehyde solution 8%, initiating monomer acrylamide 8% and sodium acrylate 2%, acryloyloxyethyltrimethylammonium chloride 2% and N,N '-methylenebisacrylamide 0.5%, curing agent ammonium sulfamate 0.02%, and the rest is water.
[0033] Under stirring conditions, gelatinize 4g of corn starch in water at 80°C for 1.5 hours in a container, adjust its pH value to 8 after starch gelatinization, adjust its temperature to 80°C, and keep it at a constant temperature for 50 minutes, then proceed according to the proportion Add potassium persulfate, sodium bisulfite, melamine, aqueous formaldehyde, ammonium sulfamate, acryloyloxyethyltrimethylammonium chloride, N,N'-methy...
Embodiment 3
[0036] A kind of high-strength jelly for snubbing operation provided by the present invention, wherein the weight percent of each component is: potato starch 4%, oxidation-reduction initiator potassium persulfate 0.5% and sodium bisulfite 0.2%, alternating Linking agent A amino resin 10%, crosslinking agent B glutaraldehyde 8%, initiator monomer acrylamide 7% and sodium acrylate 5%, N-methylol acrylamide 2%, N,N'-methylenebis Acrylamide 0.5%, curing agent ammonium chloride, and the rest is water.
[0037] Under stirring conditions, gelatinize 2.2g of potato starch in water at 75°C for 2 hours in a container. Add potassium persulfate, sodium bisulfite, amino resin, glutaraldehyde, acrylamide, sodium acrylate, N-methylolacrylamide, N,N'-methylenebisacrylamide and ammonium chloride in sequence and stir well , continue to stand at the above temperature for 90 minutes to form a gel.
[0038] The obtained colloid has a viscosity of 29000mPa.s and a maximum plugging pressure of 13....
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