Production method of synchronously extracting tea-seed oil and tea saponin from tea seed cakes
A technology of synchronous extraction and production method, which is applied in the field of synchronous extraction of tea seed oil and tea saponin from tea seed cake, which can solve the problems of large equipment investment, high production cost, and large energy consumption
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Embodiment 1
[0064] Such as figure 1 and figure 2 as shown, figure 1 A process block diagram of a production method for synchronously extracting tea seed oil and tea saponin from a tea seed cake proposed by the present invention, figure 2 It is a simplified process flow diagram of a production method for synchronously extracting tea seed oil and tea saponin from tea seed cake proposed by the present invention.
[0065] refer to figure 1 and figure 2 , a kind of tea seed cake synchronously extracting the production method of tea seed oil and tea saponin that the present invention proposes, comprises the steps:
[0066] S1. Multi-stage countercurrent pulse extraction: put the tea seed cake into the extractor, and at 55°C, first spray and soak the extraction agent containing tea seed oil with a mass fraction of 20wt%, and then separately pass the tea seed cake The mass fraction of oil is 16wt%, 12wt%, 8wt%, 4wt%, 2wt%, 0.8wt%, 0wt% extracting agent carries out eight-stage spray soakin...
Embodiment 2
[0080] A kind of production method that tea seed cake synchronously extracts tea seed oil and tea saponin that the present invention proposes comprises the following steps:
[0081] S1. Multi-stage countercurrent pulse extraction: at 50°C, first spray and soak the extraction agent containing tea seed oil with a mass fraction of 18wt%, and then extract with tea seed oil with a mass fraction of 15wt% and 11wt%, respectively. , 7wt%, 3wt%, 1.5wt%, 0.5wt%, and 0wt% of the extractant are sequentially subjected to eight-stage spray soaking extraction, and the extraction is 90min to obtain a mixed solution and a mixed solid; wherein, the mass ratio of the extractant to the tea seed cake 1.6:1, the extractant is composed of methanol and n-hexane with a mass ratio of 0.6:1;
[0082] S2, liquid separation and separation: the mixed solution obtained in S1 is filtered and separated to obtain a first mixed solution composed of tea seed oil and n-hexane and a second mixed solution composed ...
Embodiment 3
[0095] A kind of production method that tea seed cake synchronously extracts tea seed oil and tea saponin that the present invention proposes comprises the following steps:
[0096] S1. Multi-stage countercurrent pulse extraction: put the tea seed cake into the extractor, and at 60°C, first spray and soak the extraction agent containing tea seed oil with a mass fraction of 22wt%, and then separately pass the tea seed cake The mass fraction of oil is 17wt%, 13wt%, 9wt%, 5wt%, 3wt%, 1wt%, 0wt% extractant is subjected to eight-stage spray soaking extraction successively, extraction 150min, obtains mixed solution and mixed solid; The mass ratio of the extraction agent to the tea seed cake is 1.2:1, and the extraction agent is composed of methanol and n-hexane in a mass ratio of 0.8:1;
[0097] S2, liquid separation and separation: the mixed solution obtained in S1 is filtered and separated to obtain a first mixed solution composed of tea seed oil and n-hexane and a second mixed so...
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