Nitrogen-doped anatase TiO2 nano-sheet multilevel ball and preparation method thereof
A technology of nano-sheets and anatase, applied in the field of nitrogen-doped anatase TiO2 nano-sheet multi-level spheres and its preparation, can solve the problems of reaction system toxicity, easy pollution of the environment, strong corrosion, etc., and achieve green operation Environmental protection, high repeatability and good stability
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0031] Example 1
[0032] Step 1: Accurately measure 71 mL of isopropanol solvent into the autogenous pressure reactor, add 0.09 mL of the shape control agent diethylene triamine and 4.50 mL (0.0134 mol) isopropyl titanate solution, and stir gently for 1 min To be evenly dispersed. Add accurately weighed 0.0492g (0.00164mol) urea to the above mixed solution, stir slowly for 1 minute and then ultrasonically disperse for 5 minutes;
[0033] Step 2: The above-mentioned reaction kettle containing the reaction mixture is sealed and placed in an oven at 200°C to crystallize the solution in the autoclave under autogenous pressure for 24 hours. After crystallization, cool to room temperature naturally, centrifuge the pale yellow slurry, wash the precipitate with absolute ethanol 4 times and dry at 60°C for 12 hours to obtain a pale yellow precursor, denoted as 0.12N-{001}TiO 2 -24, where 0.12 is the nominal molar ratio of nitrogen atoms to titanium atoms; 24 is the crystallization time;
...
Example Embodiment
[0037] Example 2
[0038] Step 1: Accurately measure 71 mL of solvent isopropanol into the autogenous pressure reactor, add 0.09 mL of the shape control agent diethylene triamine and 4.50 mL (0.0134 mol) isopropyl titanate solution, and stir gently 1min to uniform dispersion. Add accurately weighed 0.12g (0.0041mol) of urea into the above mixed solution, stir slowly for 1 minute and then ultrasonically disperse for 5 minutes;
[0039] Step 2: The above-mentioned reaction kettle containing the reaction mixture is sealed and placed in an oven at 200°C, so that the solution in the high-pressure reaction kettle is crystallized under autogenous pressure for 24 hours. After crystallization, cool to room temperature naturally, centrifuge the light yellow slurry, wash the precipitate with absolute ethanol 4 times and dry at 60°C for 12 hours to obtain a light yellow multi-level structure precursor, denoted as 0.3N-{001}TiO 2 -24, where 0.3 is the nominal molar ratio of nitrogen atoms to t...
Example Embodiment
[0041] Example 3
[0042] Step 1: Accurately measure 71 mL of solvent isopropanol into the autogenous pressure reactor, add 0.09 mL of the shape control agent diethylene triamine and 4.50 mL (0.0134 mol) isopropyl titanate solution, and stir gently 1min to uniform dispersion. Add accurately weighed 0.4920g (0.0164mol) urea into the above mixed solution, stir slowly for 1 minute and then ultrasonically disperse for 5 minutes;
[0043] Step 2: The above-mentioned reaction kettle containing the reaction mixture is sealed and placed in an oven at 200°C to crystallize the solution in the autoclave under autogenous pressure for 24 hours. After crystallization, cool to room temperature naturally, centrifuge the light yellow slurry, wash the reaction precipitate with absolute ethanol 4 times and dry at 60°C for 12 hours to obtain a light yellow hierarchical structure precursor, denoted as 1.2N-{001}TiO 2 -24, where 1.2 is the nominal molar ratio of nitrogen atoms to titanium atoms; 24 is ...
PUM
Property | Measurement | Unit |
---|---|---|
Length | aaaaa | aaaaa |
Thickness | aaaaa | aaaaa |
Size | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap