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Sunscreen composition containing layered composite metal hydroxide and preparation method thereof

A hydroxide, layered composite technology, applied in cosmetic preparations, preparations for skin care, cosmetics, etc., can solve the problems of obvious photocatalytic effect of inorganic UV blocking materials and unsatisfactory UV shielding broad spectrum of nano titanium dioxide, etc. Achieve good compatibility, improve sun protection range and degree of sun protection, and good repeatability

Inactive Publication Date: 2015-07-29
BEIJING TECHNOLOGY AND BUSINESS UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] One of the technical problems to be solved by the present invention is to provide a sunscreen composition material containing layered composite metal hydroxide, which can solve the problem of obvious photocatalytic effect of existing inorganic ultraviolet blocking materials, and at the same time solve the problem of nano-titanium dioxide shielding UV Broad-spectrum is not ideal for technical issues

Method used

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  • Sunscreen composition containing layered composite metal hydroxide and preparation method thereof
  • Sunscreen composition containing layered composite metal hydroxide and preparation method thereof
  • Sunscreen composition containing layered composite metal hydroxide and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] 1. Composition in parts by mass of each component of the sunscreen composition:

[0019]

[0020] 2. Wherein the preparation method of the modified layered magnesium hydroxide / aluminum hydroxide composite is as follows:

[0021] (1) Co-precipitation method to prepare magnesium-aluminum type layered composite metal hydroxide:

[0022] a. 0.015mol of solid Mg(NO 3 ) 2 ·6H 2 O and 0.0075mol of solid Al(NO 3 ) 3 9H 2 O dissolved in 50mL to remove CO 2 of deionized water;

[0023] b. Dissolve 0.0625mol NaOH in 50mL to remove CO 2 of deionized water;

[0024] c. the alkali solution prepared by step b is placed in a four-necked bottle, 2 Stir vigorously under the condition of air protection, and at the same time, slowly add the salt solution prepared in step a into the four-necked bottle for about 0.5h. After the addition is completed, adjust the pH value to 8 with 5mol / L NaOH solution , 60 ℃ water bath reaction for 24h, with CO removal 2 The deionized hot water...

Embodiment 2

[0036] 1. Composition in parts by mass of each component of the sunscreen composition:

[0037]

[0038] 2. The preparation method of the modified layered zinc hydroxide / aluminum hydroxide composite is as follows:

[0039] (1) Preparation of layered zinc hydroxide / aluminum hydroxide composite by urea method:

[0040] a. Add 0.024mol of solid Zn(NO 3 ) 2 ·6H 2 O and 0.012mol of solid Al(NO 3 ) 3 9H 2 O and 0.10mol urea were dissolved in 70mL of deionized water, and stirred by magnetic force for 30 minutes;

[0041] b. In a 90 ml polytetrafluoroethylene pressure reaction vessel, crystallize at 130°C for 12 hours, centrifugally wash with deionized water until the pH is about 7, and dry at 70°C for 12h to obtain layered zinc hydroxide / Aluminum hydroxide complex;

[0042] (2) Wet-modified layered zinc hydroxide / aluminum hydroxide composite

[0043] Dilute the layered zinc hydroxide / aluminum hydroxide composite filter cake with three times its volume of deionized water ...

Embodiment 3

[0053] 1. Composition in parts by mass of each component of the sunscreen composition:

[0054]

[0055] 2. Preparation of layered zinc hydroxide / aluminum hydroxide composite by urea method:

[0056] a. Add 0.024mol of solid Zn(NO 3 ) 2 ·6H 2 O and 0.012mol of solid Al(NO 3 ) 3 9H 2 O and 0.10mol urea were dissolved in 70mL of deionized water, and stirred by magnetic force for 30 minutes;

[0057] b. In a 90 ml polytetrafluoroethylene pressure reaction vessel, crystallize at 130°C for 12 hours, centrifugally wash with deionized water until the pH is about 7, and dry at 70°C for 12h to obtain layered zinc hydroxide / Aluminum hydroxide complex.

[0058] 3. Preparation of sunscreens comprising sunscreen compositions

[0059] formula:

[0060]

[0061]

[0062] Process:

[0063] a. Add deionized water into the beaker, sprinkle Stabileze QM powder under good stirring, stir until uniform, then add other components in phase B in turn, ultrasonic for 15min, ultrason...

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Abstract

The invention discloses a sunscreen composition containing layered composite metal hydroxide and a preparation method thereof. The composition comprises the following components in parts by weight: 0.5-10 parts of layered composite metal hydroxide, 5-8 parts of ethylhexyl methoxycinnamate, 1-2 parts of butyl methoxyl dibenzoylmethane, 1-3 parts of benzophenone-3 and 0-1 part of bis-ethylhexyloxyphenol methoxyphenyl triazine, wherein the layered composite metal hydroxide material is safe, high in light stability and good in compatibility with other components, and the compatibility with other components in cosmetics is increased; the ethylhexyl methoxycinnamate and the benzophenone-3 absorb ultraviolet rays of a UVB wave band mainly, the butyl methoxyl dibenzoylmethane absorbs ultraviolet rays of a UVA wave band mainly, and the bis-ethylhexyloxyphenol methoxyphenyl triazine is a broad-spectrum UV absorbent; the layered composite metal hydroxide reaches the effect of physical screening through scattering and diffuse reflection of UV light, and realizes synergistic interaction with other organic ultraviolet absorbent with each other, so that the sunscreen range and sunscreen degree can be obviously promoted.

Description

technical field [0001] The invention belongs to the technical field of care product materials, and in particular provides a sunscreen composition containing layered composite hydroxide and a preparation method thereof, which are mainly used in the field of sunscreen cosmetics. Background technique [0002] The earth on which human beings live, due to the protection of the atmospheric ozone layer, blocks 99% of the ultraviolet radiation in the sun, so that all creatures on the earth are protected from strong ultraviolet rays. However, with the development of industrial civilization, the ozone layer has been greatly damaged, which has greatly increased the ultraviolet rays irradiated on the earth's surface and posed a serious threat to human health. The damage of UV light to epidermal cells is divided into two types: direct and indirect. UVC (220-280nm), UVB (280-320nm), and some UVA (320-400nm) can directly damage epidermal cell DNA, while most of UVA can directly reach the s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K8/49A61K8/19A61Q17/04
Inventor 王心蕊唐丽萍李勇周威李姝静
Owner BEIJING TECHNOLOGY AND BUSINESS UNIVERSITY
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