Super-soft superfine polyester fiber and preparation method thereof
An ultra-fine polyester fiber, ultra-soft technology, applied in the direction of fiber type, fiber treatment, dyeing method, etc., can solve the problems of poor tow cohesion, difficult to apply oil, difficult to adhere oil evenly, etc., to reduce surface tension, Improved smoothness, soft gloss effect
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Embodiment 1
[0053] A method for preparing ultra-soft and ultra-fine polyester fibers. Firstly, an oiling oil is prepared. The specific preparation steps are: blending the initiator butanol and strong alkali potassium hydroxide, then heating up to 105°C, and then adding Ethylene oxide, [(1,1,2,2-tetrafluoroethoxy) methyl] oxirane and propylene oxide mixed uniformly, the amount of butanol is ethylene oxide, [(1, 1,2,2-tetrafluoroethoxy) methyl] 1‰ of the total mass of ethylene oxide and propylene oxide, the amount of strong alkali potassium hydroxide is ethylene oxide, [(1,1,2, 1‰ of the total mass of 2-tetrafluoroethoxy)methyl]oxirane and propylene oxide, ethylene oxide, [(1,1,2,2-tetrafluoroethoxy)methyl]ring The molar ratio of ethylene oxide and propylene oxide is 10:1:20, the polymerization reaction is carried out under the protective atmosphere of nitrogen, the reaction pressure is 0.4MPa, and after the relative molecular weight is 1000, the fluorine-containing polyether is obtained. ...
Embodiment 2
[0068] A method for preparing ultra-soft and ultra-fine polyester fibers. Firstly, an oiling oil is prepared. The specific steps are: blend the starter butanol and strong alkali sodium hydroxide, then raise the temperature to 125°C, and then add and mix evenly The amount of ethylene oxide, [(1,1,2,2-tetrafluoroethoxy) methyl] ethylene oxide and propylene oxide, the amount of butanol is ethylene oxide, [(1,1, 2,2-tetrafluoroethoxy) methyl] 5‰ of the total mass of ethylene oxide and propylene oxide, the amount of strong alkali sodium hydroxide is ethylene oxide, [(1,1,2,2- 5‰ of the total mass of tetrafluoroethoxy)methyl]oxirane and propylene oxide, ethylene oxide, [(1,1,2,2-tetrafluoroethoxy)methyl]oxirane The molar ratio of alkane and propylene oxide is 20:3:30, the polymerization reaction is carried out under the protective atmosphere of inert gas atmosphere, the reaction pressure is 0.5MPa, and after the relative molecular weight is 4000, neutralization, adsorption and vacuu...
Embodiment 3
[0082] A preparation method of ultra-soft and ultra-fine polyester fiber. Firstly, an oiling oil is prepared. The specific steps are: blend the starter butanol and strong alkali sodium hydroxide, then raise the temperature to 115°C, and then add and mix evenly The amount of ethylene oxide, [(1,1,2,2-tetrafluoroethoxy) methyl] ethylene oxide and propylene oxide, the amount of butanol is ethylene oxide, [(1,1, 2,2-tetrafluoroethoxy) methyl] 2‰ of the total mass of ethylene oxide and propylene oxide, the amount of strong alkali sodium hydroxide is ethylene oxide, [(1,1,2,2- 1.5‰ of the total mass of tetrafluoroethoxy)methyl]oxirane and propylene oxide, ethylene oxide, [(1,1,2,2-tetrafluoroethoxy)methyl]oxirane The molar ratio of alkanes and propylene oxide is 12:1:30, the polymerization reaction is carried out under the protective atmosphere of inert gas atmosphere, the reaction pressure is 0.8MPa, and after the relative molecular weight is 3000, neutralization, adsorption and va...
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