Synergistic Acid Degradation of Corn Stalks by Microwave and Ultrasonic
A technology of corn stalks and corn stalk powder, which is applied in the field of microwave and ultrasonic synergistic acid degradation of corn stalks, which can solve the problems of high temperature and pressure resistance requirements, difficult to degrade corn stalks, and low yield of reducing sugars, reaching the reaction temperature low cost, energy saving and high efficiency in the preparation process, and low preparation cost
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Embodiment 1
[0016] The method for microwave and ultrasonic synergistic acid degradation of corn stalks of the present invention, its operating steps are as follows:
[0017] a. Pretreatment: removing impurities, purifying, drying and pulverizing the corn stalks to make 30-mesh corn stalk powder;
[0018] b. Feeding: impregnate the corn stalk powder prepared in step a with a sulfuric acid solution with a mass concentration of 1%, and the ratio of solid to liquid is 1:30g / mL;
[0019] c. Degradation: Immerse the liquid in step b for 10 minutes at a temperature of 60-90°C, start microwave and ultrasonic waves, and powers of 20W and 600W respectively, and take the liquid to complete the degradation.
Embodiment 2
[0021] The method for microwave and ultrasonic synergistic acid degradation of corn stalks of the present invention, its operating steps are as follows:
[0022] a. Pretreatment: removing impurities, purifying, drying and pulverizing the corn stalks to make 60-mesh corn stalk powder;
[0023] b. Feeding: impregnate the corn stalk powder prepared in step a with a sulfuric acid solution with a mass concentration of 5%, and the ratio of solid to liquid is 1:80g / mL;
[0024] c. Degradation: Immerse the material solution in step b for 50 minutes at a temperature of 90°C, start microwave and ultrasonic waves, and power 100W and 1000W respectively, and take the liquid to complete the degradation.
Embodiment 3
[0026] The method for microwave and ultrasonic synergistic acid degradation of corn stalks of the present invention, its operating steps are as follows:
[0027] a. Pretreatment: removing impurities, purifying, drying and pulverizing the corn stalks to make 40-mesh corn stalk powder;
[0028] b. Feeding: impregnate the corn stalk powder prepared in step a with a sulfuric acid solution with a mass concentration of 2%, and the ratio of solid to liquid is 1:40g / mL;
[0029] c. Degradation: Immerse the material liquid in step b for 20 minutes at a temperature of 70°C, start microwave and ultrasonic waves, and powers of 730W and 00W respectively, and take the liquid to complete the degradation.
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