The invention belongs to the technical field of nano-
fiber materials, in particular to a pure carbon
fiber material adopting a 'vesical string' structure and a preparation method of the pure carbon
fiber material. The preparation method comprises the following steps: preparing a
spinning solution from a spinnable
polymer material, and preparing nanofibers of uniform structures with an electrostatic
spinning device; uploading
iron oxide hydroxide cambiform nanorods on the surfaces of the nanofibers uniformly via a water bath or hydrothermal method; soaking an
iron oxide hydroxide-modified fiber membrane in a
dopamine solution, and controlling the thickness of a polydopamine
coating layer by adjusting the concentration of the
dopamine solution and the reaction time; carrying out high-temperature
carbonization treatment, so as to realize fiber
carbonization, and conversion of
iron oxide hydroxide to ferroferric
oxide as well as polydopamine to a N-
doped carbon material; removing ferroferric
oxide via soaking in an acid solution. The preparation method is safe and
environmentally friendly; the prepared pure carbon fiber material is high in
nitrogen content, specific surface area and electric
conductivity, and stable in physical and chemical properties, so as to be an ideal
electrode material for production of
new energy devices such as a
supercapacitor.